Subscriber access provided by ECOLE NORMALE SUPERIEURE LYON Article Dynamic Nuclear Polarization of Amyloidogenic Peptide Nanocrystals: GNNQQNY, a Core Segment of the Yeast Prion Protein Sup35p iMR Advanced Training Workshop I Patrick C. A. van der Wel, Kan-Nian Hu, Jzef Lewandowski, and Robert G. Griffin J. Am. Chem. Soc., 2006, 128 (33), 10840-10846• DOI: 10.1021/ja0626685 • Publication Date (Web): 02 August 2006 ApplicationsDownloaded of fromDynamic http://pubs.acs.org Nuclear on April 27, 2009 Polarisation DNP no DNP More About This Article Józef Lewandowski Additional resources and features associated with this article are available within the HTML version: April 10 2013 • Supporting Information • Links to the 13 articles that cite this article, as of the time of this article download • Wednesday,Access 10 April to 13 high resolution figures • Links to articles and content related to this article • Copyright permission to reproduce figures and/or text from this article Journal of the American Chemical Society is published by the American Chemical Society. 1155 Sixteenth Street N.W., Washington, DC 20036 2/2/2011 2/2/2011 Why to do DNP? Why bother? MR3 Advanced Topics in MR Lectures 5 and 6: Dynamic Nuclear Polarisation 13C image DNP 13C-lactate .. Walter Kockenberger,Dissolution DNP
[email protected] pressure cooker solvent (H O) 100 – 140°C 2 2 – 10 bar chase gas (Helium) (injected) (newly synthesised) 2 – 5 bar • more signal Klaes Golman et al • polarizer faster acquisition • new, previously not possible applications,sample cup now within the reach Wednesday, 10 April 13 Why bother? What’s on the plate? • Sensitivity and spin polarisation • Relevant spin interactions • The spin Hamiltonian for liquid state • Energy levels and populations I • The Solomon equations T.