CortecNet – The global NMR supplier 2 out of 40 Contact & Ordering information CONTACT & ORDERING INFORMATION 1. Minimum order is : 300 ¼ HT. 2. Shipping conditions: - 25 ¼ HT if order < 600 ¼ HT ; - free of charges if order > 600 ¼ HT ; 3. No Special Conditions for Bruker. 4. Payment terms : 30 days net. PLEASE INQUIRE FOR BIG QUANTITY TO GET SPECIAL PRICES Sincerely, Philippe Corcos [email protected] CortecNet 110, Rue de Rivoli 75001 Paris Tel : 33 1 53 40 99 20 Fax : 33 1 53 40 89 20 CortecNet – 110, rue de Rivoli – 75001 PARIS – France Tél : 33 (0)1 53 40 99 20 / Fax : 33 (0)1 53 40 89 20 e-mail : [email protected] or [email protected] / web site : http://www.cortecnet.com CortecNet – The global NMR supplier Summary 3 out of 40 SUMMARY Contact & Ordering Information 2 Summary 3 Bruker products 4 - Solid NMR and HR MAS Consumables 4 - Liquid NMR Consumables 10 - NMR Probe Accessories 19 - EPR Probe Accessories 25 - Minispec Consumables 26 - NMR General Accessories 27 - IR Accessories 31 Technical data and Helpful information 33 - Properties of Rotor and Cap Materials 34 - Speed rotation for MAS and HR MAS rotors 34 - HR-MAS sample preparation 35 - NMR Sample Tube Specifications 37 - NMR Sample Tube Pressure / Volume Data 37 - Cleaning NMR Sample Tubes 37 - Pyrex versus Borosilicate 38 - NMR Solvent Data 39 - Selection of Susceptibility Constants 40 CortecNet – 110, rue de Rivoli – 75001 PARIS – France Tél : 33 (0)1 53 40 99 20 / Fax : 33 (0)1 53 40 89 20 e-mail : [email protected] or [email protected] / web site : http://www.cortecnet.com CortecNet – The global NMR supplier Bruker products : Solid NMR and HR MAS consumables 4 out of 40 SOLID NMR AND HR MAS CONSUMABLES SOLID NMR ROTORS AND INSERTS Product Description O.D. Other sizes Material T° range & Remarks Package contents Quantity Unit Number (mm) Max. speed Price I.D. : 1.5mm for all 2.5 mm probes 1 MAS rotor ZRO 2.5/12 (P/N : HZ05165) MAS rotor ZrO2 BL2.5 2.5 Zirconia Room [-30 to +70°C] 2 H8416 Ext. length : 12mm 2 Drive caps BL2.5 (P/N : HZ05269) 1 - 2 [ZrO2] Standard [35 kHz] Sample vol. : 12µL 2 SP1 BL2.5 rotor bottom caps (P/N : HZ05276) 3 - 5 6 - 8 9 - … I.D. : 3mm for all 4 mm probes 1 MAS rotor SI N 4/18B (P/N : HZ1663) MAS rotor Si3N4 BL4 4 Silicon nitride Variable [-150 to +150°C] 3 4 1 K1911 Ext. length : 18mm 2 Kel-f BL4 caps (P/N : H6304) [Si3N4] Standard [15 kHz] Int. length : 1 BN3 BL4 cap (P/N : H6239) 12.6mm Sample vol. : 92µL I.D. : 2.5mm for all 4 mm probes 1 MAS rotor 4/18B HS (P/N : HZ2584) MAS rotor ZrO2 BL4, HS 4 Zirconia Room [-30 to +70°C] H7615 Ext. length : 18mm 3 SP1 BL4 caps (P/N : HZ2920) 1 - 4 [ZrO2] High [18 kHz] Sample vol. : 62µL 5 - … I.D. : 3mm for all 4 mm probes 1 MAS rotor ZRO 4/18B (P/N : H6283) MAS rotor ZrO2 BL4 4 Zirconia Variable [-150 to +150°C] 2 K1910 Ext. length : 18mm 2 Kel-f BL4 caps (P/N : H6304) 1 - 4 [ZrO2] Standard [15 kHz] Int. length : 1 BN3 BL4 cap (P/N : H6239) 5 - 9 12.6mm Sample vol. : 92µL 10 - … I.D. : 3mm for all 4 mm probes 1 MAS rotor ZRO 4/18B (P/N : H6283) MAS rotor ZrO2 BL4, HT 4 Zirconia High [-150 to +250°C] 2 K1914 Ext. length : 18mm 1 Kel-f BL4 cap (P/N : H6304) 1 - 4 [ZrO2] Standard [15 kHz] Int. length : 1 MAS cap MACOR BL4 (P/N : K1935) 5 - 9 12.6mm Sample vol. : 92µL 10 - … I.D. : 6mm fot BL7 probes 1 MAS rotor SI N 7/18B (P/N : HZ1620) MAS rotor Si3N4 BL7 7 Silicon nitride Variable [-150 to +150°C] 3 4 1 K1922 Ext. length : 18mm 1 Kel-f BL7 cap with hole (P/N : H6244) [Si3N4] Standard [6 kHz] 1 Kel-f BL7 cap without hole (P/N : HZ1662) 1 BN3 BL7 cap with hole (P/N : HZ1651) CortecNet – 110, rue de Rivoli – 75001 PARIS – France Tél : 33 (0)1 53 40 99 20 / Fax : 33 (0)1 53 40 89 20 e-mail : [email protected] or [email protected] / web site : http://www.cortecnet.com CortecNet – The global NMR supplier Bruker products : Solid NMR and HR MAS consumables 5 out of 40 SOLID NMR ROTORS AND INSERTS Product Description O.D. Other sizes Material T° range & Remarks Package contents Quantity Unit Number (mm) Max. speed Price I.D. : 6mm fot BL7 probes 1 MAS rotor SI N 7/18B (P/N : HZ1620) MAS rotor Si3N4 BL7 7 Silicon nitride Variable [-150 to +150°C] 3 4 1 K1922 Ext. length : 18mm 1 Kel-f BL7 cap with hole (P/N : H6244) [Si3N4] Standard [6 kHz] 1 Kel-f BL7 cap without hole (P/N : HZ1662) 1 BN3 BL7 cap with hole (P/N : HZ1651) I.D. : 5.5mm fot BL7 probes 1 MAS rotor ZRO 7/18B (D=4) (P/N : HZ1834) MAS rotor ZrO2 BL7, HS 7 Zirconia Room [-30 to +70°C] 2 H7464 Ext. length : 18mm 3 SP1 BL7 caps (P/N : HZ1835) 1 - 4 [ZrO2] High [8 kHz] 5 - … I.D. : 6mm fot BL7 probes 1 MAS rotor ZRO 7/18B (P/N : H6241) MAS rotor ZrO2 BL7, HT 7 Zirconia High [-150 to +250°C] 2 K1912 Ext. length : 18mm 1 Kel-f BL7 cap without hole (P/N : HZ1662) 1 - 4 [ZrO2] Standard [6 kHz] 1 MAS cap MACOR BL7 (P/N : K1931) 5 - … I.D. : 6mm fot BL7 probes 1 MAS rotor ZRO 7/18B (P/N : H6241) MAS rotor ZrO2 BL7 7 Zirconia Variable [-150 to +150°C] 2 K1921 Ext. length : 18mm 1 Kel-f BL7 cap without hole (P/N : HZ1662) 1 - 4 [ZrO2] Standard [6 kHz] 1 Kel-f BL7 cap with hole (P/N : H6244) 5 - 9 1 BN3 BL7 cap with hole (P/N : HZ1651) 10 - … I.D. : 6mm for DB7/18 probes 1 MAS rotor ZRO 7/18B (P/N : H6241) MAS rotor ZrO2 DB7/18 7 Zirconia Variable [-150 to +150°C] 2 P2885 Ext. length : 18mm 1 Kel-f DB7/18 cap with hole (P/N : H6156) 1 - 4 [ZrO2] Standard [6 kHz] 1 Kel-f DB7/18 cap without hole (P/N : H6302) 5 - … 1 BN3 DB7/18 cap with hole (P/N : H6303) Rotor STRETCH 7 7 I.D. : 5mm Zirconia Variable [-150 to +150°C] for 7 mm AMS BL7 STRECH 1 B0437 Ext. length : 33mm probes [ZrO2] Standard [5 kHz] for glass sample of 5 mm Rotor STRETCH 7 7 I.D. : 5mm Zirconia Variable [-150 to +150°C] for 7 mm AMS BL7 STRECH 1 B0495 Ext. length : 33mm probes [ZrO2] Standard [5 kHz] 7 mm BL7 hermetic insert 7 Kel-f Room [-20 to +70°C] for moisture sensitive 1 top MAS rotor insert (P/N : HZ2034) 1 H6251 experiments 1 bottom MAS rotor insert (P/N : HZ2038) for BL7 rotors 1 Cylindric screw M2X20 MS (P/N : H1833) I.D. : 9mm for all 10 mm probes 1 MAS rotor 10/18B (P/N : HZ2386) MAS rotor BL10 ZrO2 10 Zirconia Variable [-150 to +250°C] H7873 Ext. length : 18mm 2 Kel-f BL10 caps (P/N : HZ03929) 1 - 4 [ZrO2] Standard [4 kHz] 1 SP1 BL10 cap (P/N : HZ04039) 5 - … 1 MAS cap MACOR BL10 (P/N : HZ04040) CortecNet – 110, rue de Rivoli – 75001 PARIS – France Tél : 33 (0)1 53 40 99 20 / Fax : 33 (0)1 53 40 89 20 e-mail : [email protected] or [email protected] / web site : http://www.cortecnet.com CortecNet – The global NMR supplier Bruker products : Solid NMR and HR MAS consumables 6 out of 40 CRAMPS ROTORS AND SPACERS Product Description O.D Other sizes Material T° range & Remarks Package contents Quantity Unit Number (mm) Max. speed Price H7359 MAS rotor CRAMPS Kel-f 4 I.D. : 3mm Kel-f Room [-20 to +70°C] for DB7/18 probes 1 MAS rotor ZRO2 4/18B (P/N : H6283) 1 - 4 Ext. length : 18mm Standard [15 kHz] 1 Spacer CRAMPS BL4 Kel-f (P/N : HZ2405) with spacer HZ2405 2 Kel-f BL4 caps (P/N : H6304) 5 - 9 1 Cylindric screw M2X25 MS (P/N : H5202) 10 - … MAS rotor CRAMPS PE 4 I.D. : 3mm PE Room [-20 to +70°C] for all 4 mm probes 1 MAS rotor ZRO2 4/18B (P/N : H6283) 1 H7358 Ext. length : 18mm 1 Spacer CRAMPS BL4 PE (P/N : HZ2245) with spacer HZ2245 [Polyethylene Standard [15 kHz] ] 2 Kel-f BL4 caps (P/N : H6304) 1 Cylindric screw M2X25 MS (P/N : H5202) H7360 MAS rotor CRAMPS PTFE 4 I.D. : 3mm PTFE Room [-20 to +70°C] for all 4 mm probes 1 MAS rotor ZRO2 4/18B (P/N : H6283) 1 Ext. length : 18mm [Teflon] Standard [15 kHz] 1 Spacer CRAMPS BL4 PTFE (P/N : HZ1872) with spacer HZ1872 2 Kel-f BL4 caps (P/N : H6304) 1 Cylindric screw M2X25 MS (P/N : H5202) HZ2405 Spacer CRAMPS BL4 Kel-f 4 Kel-f Room [-20 to +70°C] for MAS CRAMPS rotor BL4 only 1 RM Kel-f RD (P/N : 19333) 1 HZ2245 Spacer CRAMPS BL4 PE 4 PE Room [+10 to +50°C] for MAS CRAMPS rotor BL4 only 1 RM PE round (P/N : 65424) 1 [Polyethylene ] HZ1872 Spacer CRAMPS BL4 PTFE 4 PTFE Room [+10 to +50°C] for MAS CRAMPS rotor BL4 only 1 RM PTFE round (P/N : 55278) 1 [Teflon] K1921CR MAS rotor CRAMPS Kel-f 7 I.D.