<p>Class: Chem Organic Experiments 1st Semester 2013/9/17 Date Order Contents page CA CB CC</p><p>1 9/17 9/17 9/17 Safety and Note in the Laboratory 1 2 9/24 9/26 9/27 MSDS introduction & Check in & Cleaning To Learn and Assemble the Apparatus for S.D. 3 10/1 10/3 10/4 Calibration of Thermometer 8 Synthesis of Ethanol by Fermentation of Sucrose 23 Distillation 10</p><p>4 10/8(AB) haliday 10/11(BC) Simple Distillation of Fermentation of Sucrose 5 10/15 10/17 10/18 Fractional Distillation of S.D. Distillate 6 10/22 10/24 10/25 Melting Point & Sublimation 30 Melting Points of Pure Urea and Cinnamic Acid Melting Points of Urea -Cinnamic Acid Mixtures Unknowns Sublimation of Naphthalene 7 10/29 10/31 11/1 Crystallization 43 Crystallization of Impure Phthalic Acid, Acetanilide and Benzoic acid 8 11/5 11/7 11/8 Thin-Layer Chromatography 61 Fluorene and Fluorenone 9 11/12 11/14 11/15 Column Chromatography 72 Separation of Fluorene and Fluorenone 10 11/19 11/21 11/22 Discussion 11 11/26 11/28 11/29 Extraction 82 Separation of Acidic and Neutral Substances 12 12/3 12/5 12/6 Nucleophilic Substitution Reaction (Mid-term) 98 Conversion of Alcohols to Alkyl Halides ; Preparation of tert-Butyl Chloride 13 12/10 12/12 12/13 Elimination 112 Preparation of Cyclohexene from Cyclohexanol 14 12/17 12/19 12/20 The Reaction of Alkenes 120 Hydration of Alkenes to Alcohols ; Preparation of Cyclohexanol 15 12/24 12/26 12/27 Infrared Spectroscopy & Chemical Test & Final Cleaning</p><p>Identification of Product of Experiment 9 by FT/IR 127 Lucas Test: Analysis of Hydroxyl Group 110 16 12/31 1/2 1/3 Discussion 17 1/7 1/9 1/10 Final Examination Practical Operation </p>