<p> Hellenic Accreditation System </p><p>Annex F1/A12 to the Certificate No. 142-4 SCOPE of ACCREDITATION of the B΄ Chemical Service of Athens of the General Chemical State Laboratory</p><p>Materials / Products Types of test / Properties to be Applied methods / Techniques to be used to be tested measured </p><p>Chemical tests</p><p>Method code 13 01 F 01 1.Fertilizers 1. Gravimetric determination of Reg. 2003/2003/EU water soluble phosphorous ΕLOT EN 15958, 15959 Method code 13 01 Α 01 2. Determination of ammoniacal Reg. 2003 / 2003/EU, nitrogen ELOT EN 15475:2010 3. Determination of nitrate nitrogen Method code 13 01 Α 02 and total nitrate and Reg. 2003 / 2003 EU, ammoniacal nitrogen ELOT EN 15476:2009 4. Determination of water-soluble Method code 13 01 K 01 potassium In house validated method, based on Reg. 2003/2003/EU M.4.1 ( flamephotometry ) 5. Determination of ureic nitrogen Method code 13 01 Α 03, Reg. 2003/2003 EU, ELOT EN 15604:2009 6. Determination of chloride Method code 13 01 CHL 01 Modified method, based on Reg. 2003/2003/EU Annex III – M.6 and IV-M.6.1 7. Gravimetric determination of Method code 13 01 F 02 soluble in inorganic acids Modified method, based on Reg. phosphorous 2003/2003/EU ELOT EN 15956, 15959 8. Gravimetric determination of the Method code 13 01 S 01 water soluble and total sulphur Reg. 2003/2003/ΕU (sulfate form) ELOT EN 15960, 15961, 15749</p><p>Page 1 of 4 Annex F1/A12 to the Certificate ESYD No.142-4 28.06.2016 Materials / Products Types of test / Properties to be Applied methods / Techniques to be used to be tested measured 9. Gravimetric determination of the Method code 13 01 F 03 neutral ammonium citrate soluble Reg. 2003/2003/ΕU phosphorous ELOT EN 15957, 15959</p><p>Method code 13 02 KAD 01 2. Plastics 1. Determination of total cadmium in In house validated method, FAAS* plastics</p><p>Method code 13 02 PTH 01 2. Identification of phthalate esters in In house validated method, HPLC PVC articles 3. Identification and quantification of Method code 13 04 DEHP_1 Di[2-ethylhexyl]phthalate in In house validated method, GC-MS PVC materials 3. Paper and 1. Determination of paper and Method code 13 02 04 ISO 2144: 2015 paperboard paperboard ash on ignition at 900OC ISO 287:2009 ISO 638:2008 2. Determination of pH of aqueous Method code 13 02 07 extracts-Part 1 : Cold extraction ISO 6588-1:2012 ISO 186:2002 Physical tests</p><p>1. Fabrics 1. Textiles – Tests for colour Method code 13 03 04 fastness-Part-C10: Colour fastness to ISO 105-C10 : 2006 washing with soap or soap and soda. 2. Textiles - Colour fastness to Method code 13 03 05 moderate washing: (60±2)oC Y-333/69 (ed. General Army Staff) 3. Textiles - Colour fastness to Method code 13 03 02 perspiration ISO 105-Ε04: 2013 4. Textiles - Colour fastness to water Method code 13 03 03 ELOT EN ISO 105-E01:2013 5. Textiles - Colour fastness to dry Method code 13 03 06 cleaning using ELOT EN ISO 105-D01:2011 perchloroethylene solvent Mechanical tests</p><p>1. Paper and board 1. Determination of thickness of Method code 13 02 02 single sheets of paper and paper Modified method based on standard ELOT EN board ISO 534: 2012 and ISO 187: 1990</p><p>2. Determination of tensile strength Method code 13 02 03 of paper and paperboard Modified method based on standard ISO 1924- 2:2008 and ISO 187:1990 3. Determination of smoothness Method code 13 02 05, (Bekk) of paper and paper board Modified method based on standard ISO 5627:1995, ISO 187:1990</p><p>Page 2 of 4 Annex F1/A12 to the Certificate ESYD No.142-4 28.06.2016 Materials / Products Types of test / Properties to be Applied methods / Techniques to be used to be tested measured </p><p>4. Determination of Method code 13 02 06, roughness/smoothness (air leak Modified method based on standard ISO 8791- 1. Paper and board method) of paper and paper board 2: 2013 and ISO 187:1990 (cont.)</p><p>Chemical tests</p><p>1. Materials and 1. Determination of Overall Method Code: ΟΜ-GRAV articles intended to Migration from plastics Documented in-house method, come into contact indented to come in contact based on European standards: with food. with food, into volatile food Α. ΕΛΟΤ EN 1186-1/2002, by Gravimetry stimulants, by Gravimetry. Β. ΕΛΟΤ EN 1186-3/2002, by Gravimetry Γ. ΕΛΟΤ EN 1186-5/2002, by Gravimetry Δ. ΕΛΟΤ EN 1186-9/2002, by Gravimetry Ε. ΕΛΟΤ EN 1186-14/2002, by Gravimetry ΣΤ. ΕΛΟΤ EN 1186-15/2002, by Gravimetry Method Code: OM10 2. Determination of Overall Documented in-house method Migration from plastics, indented to based on European standards: come into contact with food, into ELOT EN 1186-2:2002 food simulant D (vegetable oil) 2 ΕΛΟΤ EN ISO 1186-8/2002 ΕΛΟΤ EN ISO 1186-13/2002 by Gravimetry/Gas Chromatography 3. Determination of the Method Code: EM1 concentration of DEHA and DEHP Documented in-house method into plastics from PVC. based on J. of Chromatography (1987), 387 509-514, by Gas Chromatography 4. Determination of Specific Method Code: EM2 Migration of DEHA and DEHP from Documented in-house method plastics into isooctane based on J. of Chromatography (1997), 387 509-514, by Gas Chromatography Method Code: EM3 5. Determination of Specific Documented in-house method Migration of DEHA and DEHP from based on J. of Chromatography plastic films into refined olive oil (1987), 387 509-514, by Gas Chromatography 6. Semi-quantitative estimation of Method Code: EM4 specific migration from plastics. Documented in-house method based on CEN TC194/SC1/WG2: N 118, D. van Battum and J.B.H. van Lierop, by Gas Chromatography. 7. Determination of Specific Method Code: EM11 Migration of 2,2 Bis(4- Documented in-house method Hydroxyphenyl) propane in food based on BCR, MAT1-CT92-0006 simulants. final report: Annex 1, by HPLC - UV-Vis or FLD</p><p>Page 3 of 4 Annex F1/A12 to the Certificate ESYD No.142-4 28.06.2016 Materials / Products Types of test / Properties to be Applied methods / Techniques to be used to be tested measured Method Code: EM15 8. Determination of specific 1. Materials and Documented in-house method based on migration of formaldehyde and articles intended to CEN/TS 13130-23:2005 Materials and articles hexamethylenetetramine, into food come into contact in contact with foodstuffs- Plastics substances simulant B, acetic acid 3% (w/v), by with food (cont.) subject to limitation- Part 23: Determination of Spectrophotometry UV-VIS. formaldehyde and hexamethylenetetramine in food simulants. Spectrophotometry UV-VIS Method Code: EM16 9. Determination of specific Documented in-house method based on migration of melamine into food CEN/TS 13130-27:2005 Materials and articles simulant B, acetic acid 3% (w/v), by in contact with foodstuffs- Plastics substances HPLC-DAD. subject to limitation- Part 27: Determination of 2,4,6-triamino-1,3,5-triazine in food simulants. Liquide Chromatography, HPLC-DAD * FAAS: Flame Atomic Absorption Spectrometry.</p><p>Site of assessment : Permanent Laboratory Premises, 16 An. Tsocha Str., Athens, Greece. Approved signatories: Eug. Lampi, I. Xronaios, M. Stassinopoulou, M. Kormali, St. Xydas, Ar. Papageorgiou, Thras. Savvas, E. Chatiri, K. Chryssou, E.Poulima, T.Togkalidou, E.Dessipri.</p><p>This scope of Accreditation replaces the previous one dated 20.04.2016. The Accreditation Certificate No 142-4, to ELOT EN ISO/IEC 17025:2005, is valid until 06.11.2019.</p><p>Athens, July 28th, 2016</p><p>Ioannis Sitaras Director of the Laboratories Accreditation Division</p><p>Page 4 of 4 Annex F1/A12 to the Certificate ESYD No.142-4 28.06.2016</p>