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IIP , 7 17 (bds, 1H) (iii) v7 7;i/AHFAPI#ft©AGK (7) 1, 1, 1, 5, 5,5-\*V-71U*U-2-7 5 JO P (klTHHFAPi: K7) © -6-E 50g©'X*»7;i/:*n7-tzE;l/'7-t: F 7 (WTHFAfc|g7 ; £100ml© X9 J *5 7 > * =-7 a 1 1 /minOKlr* **j30£IH|g#>'*7''j >^Lfco P> ftiPLfco KSdOT’t;: J; P> SS«ETT*, W^IMBt5teMi,!)!f»?> fltz„ ro6fei6S^'>=. VP/^IFEtiSAL, 1 torr@S©i®ETT% 170X17*30 ^RfliD»>Lfc„ KfEI*Tf£, 2MC!§mtt-»Ml. SfiT-StAft^ CPfcfiKtiOHHF AP^efaftLf;. fiHmStST*#mcekP)fT&.D;f-0 lR®:31.7g, lR$:63% (7) Me2Au(HFAP):DMGHFAP©-&tit DMGHFAPti, DMGTFAPfcRSO^ftCj; P)-6-fiKL^„ IPAUlDk: ft©7kS®tCHHFAP 2.92g£^trx7/-ll/?§mOiiil£jO;L, r©f§®C&FK£Si ft. SS"C*S#>7’C«k p)SS$-@*LfcftC.Sfe®?6tttiH$-ii$ES@K«k pi ttBSLfc ($,5 ; 63~64‘C/3. 2torr) 0«*:2. 57g, 1R5$5:42X, bright yellow©® ft„ **, ; 124. 17, 1H-NMR (CDCL3) ; 51. 184ppm (s, 3fl) , 1.200 (s, 3H) , 5.6 87 (d, 1H, J (HH12.54) , 7.777 (s, 1H) , M S (m/e) : 433.