Table S1 Materials and Groups Were Used in This Study. Citrus

Table S1 Materials and Groups Were Used in This Study. Citrus

<p>Table S1 Materials and groups were used in this study. </p><ul style="display: flex;"><li style="flex:1">Citrus germplasms </li><li style="flex:1">Species name </li><li style="flex:1">Group Wild&nbsp;or Cultivar </li></ul><p>Huanongbendizao tangerine Guinongbendizao tangerine Guizhouwuhezhuju tangerine <br>Red Tangerine <br>LSM LSM LSM LSM LSM LSM LSM LSM LSM LSM LSM LSM LSM LSM LSM LSM LSM LSM LSM LSM LSM LSM LSM LSM <br>Cultivar (C) <br>CC<br>Wild (W) <br>Huangyanbendizao tangerine <br>Nanfengmiju tangerine <br>Nianju tangerine <br>CCC</p><ul style="display: flex;"><li style="flex:1">Nieduyedonggan </li><li style="flex:1">W</li></ul><p></p><ul style="display: flex;"><li style="flex:1">C</li><li style="flex:1">E-gan No.1 Ponkan tangerine </li></ul><p></p><ul style="display: flex;"><li style="flex:1">Huapiju tangerine </li><li style="flex:1">C</li></ul><p>Wuhe Ponkan tangerine India sour Tangerine Wulong Sour Tangerine Cupigoushigan tangerine Dakengyeju tangerine Daoxianyeju tangerine Jiangyongyeju tangerine Mangshanju tangerine Xipigoushigan tangerine <br>Damaliu tangerine <br>CWWWWWWWWWWC<br>Loose-skin mandarin </p><p>(<em>Citrus reticulate</em>) </p><p>Yaoxianggan tangerine <br>Miyagawa Wase </p><ul style="display: flex;"><li style="flex:1">Guangmingzao </li><li style="flex:1">C</li></ul><p></p><ul style="display: flex;"><li style="flex:1">Guoqing No.4 </li><li style="flex:1">C</li></ul><p>Changyang Kamei <br>Dapu <br>LSM LSM LSM LSM LSM CCL CCL CCL CCL CCL CCL CCL CCL CCL CCL CCL CCL CCL CCL CCL CCL SW <br>CCCCCCCCCCCCCCCCCCCCCCCCCC<br>Inaba Wase Guoqing No.1 <br>Nichinan No.1 Wase Caffion clementine De nules clementine Hernadinal clementine Marisal clementine Monreal clementine Nour clementine Orograde clementine Oroval clementine Pons clementine <br>Clementine mandarin (<em>C. </em></p><p><em>reticulate × C. sinensis</em>) </p><p>Rrecoce clementine Rubino clementine Sidiaissa1 clementine <br>Spinoso.V,C,R clementine <br>SRA63 clementine SRA92 clementine Tomatera clementine <br>Anliucheng <br>Qianyang Wuhe Dahong Hamlin Sweet Orange <br>Red Anliucheng <br>SW </p><p>Sweet orange (<em>C. sinensis</em>) SW </p><p>SW </p><ul style="display: flex;"><li style="flex:1">SW </li><li style="flex:1">Meishan Wuhejincheng </li></ul><p>Taoye sweet orange <br>Xuegan <br>SW SW SW SW SW SW SW SW SW SW SW SW SW SW SW SW SW SW SW P<br>CCCCCCCCCCCCCCCCCCCCCCCCCW<br>Qingpi <br>Carter Valencia&nbsp;orange Frost Valencia orange Crame Navel Orange Palmer Navel Orange Red grand Navel Orange Roberson Navel Orange Smithearly Navel Orange Fukumoto Navel Orange Red Flesh Navel Orange Washington Naval Orange <br>Dream Navel Orange Nice navel Orange <br>Newhall Navel Orange Seike Navel Orange Xiatian Navel Orange Zaohong Navel Orange Huanonghongyou Pomelo </p><ul style="display: flex;"><li style="flex:1">Taiyou Pomelo </li><li style="flex:1">P</li></ul><p></p><ul style="display: flex;"><li style="flex:1">Acidless Pomelo </li><li style="flex:1">P</li></ul><p>Fenghuangyou Pomelo Fenghuangyou Pomelo <br>Juanpi Pomelo </p><p>Pomelo (<em>C. grandis</em>) </p><p>PPP</p><ul style="display: flex;"><li style="flex:1">Ni 800 Pomelo </li><li style="flex:1">P</li></ul><p>Kuigan Pomelo <br>Lime </p><ul style="display: flex;"><li style="flex:1">P</li><li style="flex:1">W</li></ul><p>WC<br>Lem Lem Lem Lem Lem <br>Eureka Lemon Volkamer lemon <br>Limonia </p><p>Lemon (<em>C.limon</em>) </p><p>CW</p><ul style="display: flex;"><li style="flex:1">W</li><li style="flex:1">Red Limonia </li></ul><p></p><p>Note LSM: loose-skin mandarin; CCL: clementine mandarin; SW: sweet orange; P: pomelo; Lem: lemon. </p><p>Table S2: Volatile compounds were used to PLS-DA in four citrus species. <br>Abb. C1 compounds α-pinene <br>ID SSSSSSSSSSSTTTSS<br>Abb. C46 C47 C48 C49 C50 C51 C52 C53 C54 C55 C56 C57 C58 C59 C60 C61 compounds γ-elemene <br>ID TTTTTTTTTTTS</p><ul style="display: flex;"><li style="flex:1">C2 </li><li style="flex:1">sabinene </li><li style="flex:1"><em>trans</em>-α-bergamotene </li></ul><p></p><ul style="display: flex;"><li style="flex:1">α-guaiene </li><li style="flex:1">C3 </li><li style="flex:1">β-pinene </li></ul><p></p><ul style="display: flex;"><li style="flex:1">C4 </li><li style="flex:1">β-myrcene </li><li style="flex:1">germacrene D </li></ul><p></p><ul style="display: flex;"><li style="flex:1">elixene </li><li style="flex:1">C5 </li><li style="flex:1">α-phellandrene </li></ul><p>α-terpinene d-limonene β-cis-ocimene </p><p><em>trans</em>-β-ocimene </p><p>γ-terpinene terpinolene α-thujene </p><ul style="display: flex;"><li style="flex:1">C6 </li><li style="flex:1">α-selinene </li></ul><p></p><ul style="display: flex;"><li style="flex:1">C7 </li><li style="flex:1">α-muurolene </li></ul><p></p><ul style="display: flex;"><li style="flex:1">δ-guaiene </li><li style="flex:1">C8 </li></ul><p></p><ul style="display: flex;"><li style="flex:1">C9 </li><li style="flex:1">β-bisabolene </li></ul><p></p><ul style="display: flex;"><li style="flex:1">δ-cadinene </li><li style="flex:1">C10 </li></ul><p>C11 C12 C13 C14 C15 C16 germacrene B </p><p><em>trans</em>-nerolidol </p><p></p><ul style="display: flex;"><li style="flex:1">elemol </li><li style="flex:1">camphene </li><li style="flex:1">T</li></ul><p>TTSpseudolimonen <em>cis</em>-sabinene hydrate β-linalool germacrene D-4-ol β-selinenol caryophyllene oxide <br>2,6,10-trimethyl-2,6,9,11- dodecatetraenal α-sinensal </p><ul style="display: flex;"><li style="flex:1">S</li><li style="flex:1">T</li></ul><p>C17 </p><p>C18 C19 C20 C21 C22 C23 C24 terpinen-4-ol α-terpineol <br>C62 C63 C64 C65 C66 C67 C68 C69 <br>SSSTSSS<br>TTTTTS</p><ul style="display: flex;"><li style="flex:1">nerol </li><li style="flex:1">1-octanol </li></ul><p>β-citronellol <em>cis</em>-p-mentha-2,8-dien-1-ol citronellal hexanal <br>(E)-2-hexenal octanal </p><ul style="display: flex;"><li style="flex:1">β-citral </li><li style="flex:1">nonanal </li></ul><p></p><ul style="display: flex;"><li style="flex:1">(E)-α-citral </li><li style="flex:1">decanal </li><li style="flex:1">S</li></ul><p>C25 C26 C27 C28 C29 C30 C31 C32 C33 C34 C35 C36 C37 C38 C39 C40 C41 C42 C43 C44 C45 perillal d-camphor <br>TSSTSSSSSTSSSSSTTTTTT<br>C70 C71 C72 C73 C74 C75 C76 C77 C78 C79 C80 C81 C82 C83 C84 C85 C86 C87 C88 C89 <br>(Z)-2-decenal undecanal <br>SS</p><ul style="display: flex;"><li style="flex:1">(+)-carvon </li><li style="flex:1">dodecanal </li><li style="flex:1">S</li></ul><p>(+)-p-mentha-1,8-dien-3-one <em>cis</em>-limonene oxide <em>trans</em>-limonene oxide citronellyl acetate nerol acetate </p><ul style="display: flex;"><li style="flex:1">3-hexenal </li><li style="flex:1">T</li></ul><p>TSn-hexadecanoic acid methyl palmitate butyl acetate acetic acid, octyl ester octyl butanoate methyl linoleate methyl oleate methyl stearate undecane <br>TTTTTTTTTTTTTTgeranyl acetate perillyl acetate caryophyllene <br>(Z)-β-farnesene α-caryophyllene </p><ul style="display: flex;"><li style="flex:1">valencene </li><li style="flex:1">dodecane </li></ul><p></p><ul style="display: flex;"><li style="flex:1">α-farnesene </li><li style="flex:1">tetradecane </li></ul><p></p><ul style="display: flex;"><li style="flex:1">δ-elemene </li><li style="flex:1">p-cymene </li></ul><p></p><ul style="display: flex;"><li style="flex:1">α-cubebene </li><li style="flex:1">thymol </li></ul><p></p><ul style="display: flex;"><li style="flex:1">copaene </li><li style="flex:1">methyl thymyl ether </li></ul><p></p><ul style="display: flex;"><li style="flex:1">nootkatone </li><li style="flex:1">β-cubebene </li></ul><p></p><ul style="display: flex;"><li style="flex:1">β-elemene </li><li style="flex:1">limettin </li></ul><p><em>cis</em>-α-bergamotene </p><p>Note T: tentatively identified compounds; S:compounds identified based on authentic standards. </p><p>Table S3: The potential biomarkers were selected in Clementine mandarin and Wild citrus germplasms. </p><p>Clementine mandarin <br>Abb. CM1 CM2 CM3 CM4 CM5 CM6 CM7 CM8 CM9 CM10 CM11 CM12 CM13 CM14 <br>Compounds <br>(Z)-β-farnesene dodecanal <br>VIP value <br>2.13 2.08 2.01 1.89 1.83 1.77 1.76 1.75 1.63 1.63 1.6 decanal α-terpineol acetate α-muurolene nerol acetate ylangene α-sinensal <em>cis</em>-p-mentha-2,8-dien-1-ol γ-terpinene <br>2,6,10-trimethyl-2,6,9,11-dodecatetraenal </p><ul style="display: flex;"><li style="flex:1">citronellal </li><li style="flex:1">1.56 </li></ul><p>1.53 1.5 sabinene allo-ocimene <br>Wild citrus germplasms </p><ul style="display: flex;"><li style="flex:1">Compounds </li><li style="flex:1">Abb. </li></ul><p>WM1 WM2 WM3 WM4 WM5 WM6 WM7 <br>VIP value </p><ul style="display: flex;"><li style="flex:1">2.26 </li><li style="flex:1">germacrene D </li></ul><p></p><p><em>trans</em>-nerolidol </p><p>germacrene B <br>2.12 2.08 </p><ul style="display: flex;"><li style="flex:1">γ-elemene </li><li style="flex:1">1.97 </li></ul><p></p><ul style="display: flex;"><li style="flex:1">β-selinenol </li><li style="flex:1">1.94 </li></ul><p>(+)-p-mentha-1,8-dien-3-one citronellyl acetate <br>1.93 1.81 <br>WM8 WM9 d-camphor β-linalool <br>1.8 1.8 <br>WM10 WM11 WM12 WM13 WM14 WM15 WM16 WM17 WM18 WM19 WM20 </p><ul style="display: flex;"><li style="flex:1">citronellal </li><li style="flex:1">1.76 </li></ul><p>1.71 1.7 </p><p><em>trans</em>-β-ocimene </p><p>α-pinene </p><ul style="display: flex;"><li style="flex:1">δ-elemene </li><li style="flex:1">1.69 </li></ul><p>1.67 1.63 1.62 1.62 1.57 1.54 1.53 β-citronellol α-thujene germacrene D-4-ol <br>3-hexenal elemol α-terpinene γ-terpinene </p><p>Figure 1<em>. </em>The contents of volatiles in CCL, LSM and SW peels. CCL: clementine mandarin; LSM: loose-skin mandarin; SW: sweet orange. The compounds were listed in the Table S3. Figure S2: The Contents of potential biomarkers in wild and cultivar germplasms. The contents of volatiles were normalized by log2. The compounds were listed in the Table S3. C: Cultivar germplasms; W: Wild citrus germplasms. </p>

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