ASM Sc. J., 13, Special Issue 4, 2020 for NCAFM2018, 45-52 The Effect of Mixing on the Aeration Structure of Kuih Bahulu Sharifah Hafiza M.R.1∗ and Norazatul Hanim M.R.2 1Engineering Research Centre, MARDI Headquarters, Persiaran MARDI-UPM, 43400 Serdang, Selangor 2Food Technology Division, School of Industrial Technology, Universiti Sains Malaysia, 11800 Minden, Pulau Pinang Aerated food is appreciated mainly due to its structure that able to produce different sensory characteristics. Kuih Bahulu can be classified as an aerated baked product in which the aeration is achieved by mechanical whipping. The aeration method was differentiated to explore the impact of mixing towards the aeration structure of Kuih Bahulu. In the manual process, a spring whisk that is bounced up and down was used, while in the automated process, a planetary mixer, with wire whip attachment was used. The highest 171% overrun was achieved from a foam of 15 minutes of automated mixing. Rheologically, both Kuih Bahulu batter showed a shear thinning behaviour, (n 1) in a range of 0.7 to 0.8. The cake produced from the automatically mixed batter had lower cake volume 563 cm3 than the manually mixed batter, the air bubbles in the batter were more compact with an average air bubbles distance 227.0 ± 62.0 µm and smaller in size with an average diameter of 140.6 ± 42.5 µm. Keywords aeration; aerated food; Kuih Bahulu; mixing I. INTRODUCTION stability. However, thermodynamically, the foam is considered unstable (Campbell & Mougeot, 1999). Bubbles Foods with bubble formations are regarded as aerated foods. may coalescence, coarsening and disproportioning (Jang et The bubbles are considered as one of the food ingredient al., 2006; Lazidis et al., 2017) (Campbell & Mougeot, 1999; Germain & Aguilera, 2014). It is known that properties of foam differ based on the Bubbles are exploited to give versatility and novel properties method and equipment used to achieve foaming (Phillips et to the final food products especially to the texture, al., 1987) and the methods to achieve aeration can also be appearance and shelf life (Campbell & Mougeot, 1999; used to categorize aerated commonly used food (Campbell & Germain & Aguilera, 2014; Jang et al., 2005; Lau & Mougeot, 1999). The simplest and most useful aeration Dickinson, 2004). Aerating food can result in a reduced in method for quantifying the foam properties (Phillips et al., the product density, change in the texture and rheology, 1990; Phillips et al., 1987) is via mechanical action or mixing. increased surface area, modification of digestibility, a Mixing of cake batter is required for combining all decrease of flavour intensity and shorter shelf life (Campbell ingredients into a homogeneous batter and stable emulsion & Mougeot, 1999; Germain & Aguilera, 2014). (Wilderjans et al., 2013). Air bubbles incorporation is also Generally all bubbles or foams initially in liquid form believed initiated at the stage of batter preparation (Brooker, (Germain & Aguilera, 2014). Foam is a colloid system, with 1993). The properties of the foam are primarily affected by water as the continuous phase and the gas bubbles (or air) the stirring parameters during mixing, for instance, impeller as the dispersed phase. The presence of interfacial surface type, mixing speed and time (Jang et al., 2005; Lomakina & tension interconnecting these two phases and lead to its Mikova, 2006; Spencer et al., 2008) and other intrinsic *Corresponding author’s e-mail: [email protected] ASM Science Journal, Volume 13, Special Issue 3, 2020 for NCAFM2018 properties such as viscosity, surface tension and the A. Mixing Parameters continuous media (Jang et al., 2005). Kuih Bahulu can be classified as an aerated baked product In the automated process, wire whisk beater was attached to in which the aeration is achieved by mechanical whipping. It a heavy duty stand mixer (Kitchen Aid Model 5K5SS, USA). is also a foam cake type similar to sponge cake, in which the The mixer speed was adjusted to speed 5, and the mixing fat content is contributed by the composition of egg yolk process was continued for 15 minutes. While in the manual (Miller, 2016). The process of making Kuih Bahulu begins process, the spring whisk beater was used, and the mixing process also continued for 15 minutes. In every fifteen with the creaming of egg and sugar and then followed by minutes of manual mixing, an average of 400 strokes of folding of flour into the mixture. These processes are beating process occurred. described as two steps, single mixing in the foam type cakes batter processing (Wilderjans et al., 2013) B. Foam Characterization Kuih Bahulu is listed as one of Malaysia intangible heritage food by the National Heritage Department (Negara, Overrun measurements of the batter were done according to 2019). Kuih Bahulu is one of the many usually snacks that the methods of Lau and Dickinson (2004); Phillips et al. are served during festive occasions and still popularly eaten (1990); Phillips et al. (1987); M. C. Tan et al. (2011) with a as everyday afternoon tea snacks to the locals (Raji et al., slight modification to prevent entrapped air pocket in the 2017). Abdul Wahid (2015) also mentioned that the effort to foam. The eggs were stirred with sugar in 1:1 ratio for 15 introduce Kuih Bahulu as one of the tourism’s food is minutes in the pre weighted stainless steel container. At hindered by the food quality. To date, there are no studies every 5 minutes interval, the foam was scooped out, filled in on the food quality aspects of this cake, except on the a cup and levelled. The mixing process was paused briefly, proximate analysis by Rosniyana et al. (2003) and the gap and the egg-whipped was then weighed. The period of perceptions analysis between producer and consumer of the pausing and resuming was minimized to 2 minutes. The cakes by Abdul Wahid (2015); Abdul Wahid and Mudor same procedures were also implemented in the manual (2016); (Mudor, 2010); Wahid (2009). process. The overrun is calculated based on Equation 1. Therefore, this study aims to compare the aeration Experiments were carried out in triplicates. structure includes foam characterization, batter density, batter rheology and images, alongside the characteristics of ρ of unaerated batter Overrun = ( − 1) × 100 (1) Kuih Bahulu such as cake volumes produced from the ρ of aerated batter automatic and manual mixing process. C. Batter Density II. MATERIALS AND METHODS Batter density was measured following the methods described by Mei C Tan et al. (2010); M. C. Tan et al. (2011). All materials were sourced from the local hypermarket A cup with a volume of 83 cm3 was used and measured at (Tesco Sg Dua, Penang). Kuih Bahulu batter was prepared room temperature. The batter was then filled in the cup, by mixing the L size eggs (38 % w/w) and granulated sugar leveled of the top surface with cautious using a spatula to (30 % w/w). Wheat flour (32 % w/w) was then folded in the prevent large air pocket trapped in the batter. It was then mixture. The batter was then filled in the mould (flower weighted in the weighing balance. The batter density, batter shaped, about 40mm diameter) and baked in the convection is measured as: oven (Bakbar Turbofan 32, New South Wales, Australia) at 180C for 20 minutes. 퐦퐚퐬퐬 퐨퐟 퐛퐚퐭퐭퐞퐫 (퐠) 훒 = (2) 퐛퐚퐭퐭퐞퐫 퐕퐨퐥퐮퐦퐞 퐨퐟 퐜퐮퐩 (퐜퐦ퟑ) 46 ASM Science Journal, Volume 13, Special Issue 3, 2020 for NCAFM2018 All experiments were carried out in triplicates in both consecutive reading. A value of 0.253 g/cm3 was then used automated and manual mixing process. as the seed density, seed for the cake density measurement. For the cake density measurement, 1000 cm3 coriander seed D. Batter Rheology was first poured in the rectangle container. A cake was then placed inside the container, and the remaining space was The rheology measurements were carried out using then again filled with coriander seeds. The surface of the Rheometer (AR1000-N, TA Instrument, New Castle, USA). container is levelled to remove excess seed and the container A cone and plate, 40 mm, 2 geometry was used to is then weighted, obtaining the Wseed. Vseed which is the characterize the steady-state flow behaviour. The shear rate volume of seeds occupying the space within the cake is 3 ramp (10 to 10 Pa) was set in the rheometer. The excess calculated by dividing the Wseed with its density, seed. The batter was removed, and silicone oil was applied to each formula is given as in Equation 4 below. In order to get the sample prior to rheology measurements to prevent drying. cake volume, Vcake, the volume of the empty container, Data of shear rate-shear stress was plotted and then fitted to Vcontainer (1440 cm3) is then subtracted with the volume of the Power Law model in Equation 3. occupied seed, Vseed. The calculation is simplified as in Equation 5. n τ = K (3) Wseed Vseed = (4) ρseed Wseed Vseed = (5) where is shear stress (Pa); is shear rate (1/s); K is ρseed consistency index (Pa.sn) and n is the flow behaviour index. K and n value were obtained from the Power Law model III. RESULTS AND linearized graph plot. DISCUSSION E. Batter Images A. Overrun Samples were freeze-dried for 48 hours at 25 C in a freeze In this experiment, the overrun was measured during the dryer (LD53, Millrock Technology, New York, USA) and creaming of egg products and sugar. Before mixing, the then followed in oven drying (ED 23, Binder, Germany). mixture was only whole eggs and sugar. After 15 minutes of Batter samples in 1x1 cm cube sizes were prepared and mixing, the foam was created.