Table S2. Matrix Effects, Linear Range, Correlation Coefficients, Recoveries, Rsds And

Table S2. Matrix effects, linear range, correlation coefficients, recoveries, RSDs and expanded uncertainties (U) of 216 pesticides QuEChERS method without clean-up step analysis by GC-µECD-NPD and GC-MS/MS.

No I Range R2 M U Re RS R RS R RS Ra R2 M U R RSD Re R Reco R . of D (mg co D ec D ec D ng e (%) co S very S E ( E (%) act kg-1) ver (%) o (%) ov (%) e c ver D (%) D ive o % y v er (m o y 100 su f (% er y g v (% ( LOQ ( ( ) ( bst ) y ( kg- e ) % % an p % ( % 1) % r 10 ) ) ce e LO % ) y LO ) ) s Q ) 10 Q t 1 0 ( i 0 L % c L O ) i O Q d Q L e O s Q GC GC-MS/MS µECD- NPD 1. 1 18 21 18 15 12 3 21 79 1 80 1 78 6 0.005 3 0.03-3.0 0.999 0.998 -0.5 4 62 65 60 2. 5 9 17 1 1 1 0.005 1 24 78 4 75 4 70 2 0.01-1.0 0.999 0.999 0 65 67 66 -0.5 5 3. 4 -3 18 3 1 1 - 23 84 3 83 3 89 3 0.005 8 0.01-1.0 0.999 0.999 1 -0.5 62 65 60 4 4. 1 -2 21 3 2 4 1 24 77 4 70 4 70 9 0.005 4 0.01-1.0 0.999 0.999 2 -0.5 1 92 87 95 5. 1 -8 21 3 1 3 - 15 92 7 79 7 82 3 0.005 7 0.02-2.0 0.999 0.999 1 -0.5 7 61 68 71 2 6. 1 0.01-1.0 0.999 - 17 60 1 61 1 62 1 0.01- 0.999 - 23 82 3 84 3 78 2 3 20 4 1.0 3 7. 1 13 25 10 14 15 5 27 81 7 95 7 90 5 0.005 4 0.05-5.0 0.999 0.994 -0.5 7 62 60 59 8. 1 47 25 7 7 9 4 28 10 8 120 8 120 1 0.005 2 0.01-1.0 0.999 0.999 8 7 -0.5 0 105 110 100 9. 1 -4 20 17 3 3 - 18 10 9 115 9 118 5 0.005 0 0.01-1.0 0.999 0.999 8 2 -0.5 8 80 78 90 10. 4 -3 16 5 3 6 0.005 - 21 70 1 70 1 69 6 0.02-2.0 0.998 0.999 4 82 73 82 -0.5 6 11. 1 18 18 2 1 2 1 27 80 12 103 12 97 3 0.005 9 0.01-1.0 0.999 0.997 -0.5 6 67 63 70 12. 8 12 22 12 8 13 0.005 1 27 70 12 75 12 93 7 0.01-1.0 0.999 0.997 8 90 85 65 -0.5 1 13. 1 31 30 14 13 14 2 24 93 9 75 9 88 4 0.005 7 0.01-1.0 0.999 0.997 4 -0.5 9 115 95 110 14. 1 24 21 4 4 2 2 28 73 13 91 5 99 6 0.005 7 0.01-1.0 0.999 0.999 8 -0.5 3 75 80 85 15. 6 0 16 2 3 1 0.005 3 25 72 15 96 6 100 1 0.01-1.0 0.999 0.999 2 58 62 60 -0.5 7 16. 7 - 18 3 4 4 0.005 6 21 70 6 72 15 81 3 0.01-1.0 0.999 0.999 2 18 95 88 96 -0.5 17. 3 -2 19 3 3 2 0.005 - 19 98 4 103 4 105 0 0.01-1.0 0.999 0.999 3 72 84 86 -0.5 7 18. 5 38 24 6 9 8 0.005 5 24 80 9 96 4 80 9 0.01-1.0 0.998 0.997 3 106 96 105 -0.5 19. 1 53 17 16 4 4 1 20 81 5 86 4 90 2 0.01- 5 0.02-2.0 0.999 0.995 0 1.0 8 104 100 106 20. 2 20 17 1 1 1 3 21 72 6 83 6 73 2 0.005 1 0.01-1.0 0.999 0.995 -0.5 3 75 76 73 21. 2 0.01-1.0 0.999 -7 23 98 3 93 6 110 5 0.005 0.999 - 10 88 1 87 2 89 8 3 1 -0.5 6 22. 1 - 16 11 1 1 - 21 76 6 65 3 68 1 0.005 6 0.01-1.0 0.999 17 0.999 7 -0.5 2 64 67 69 23. 1 -4 19 6 6 4 - 19 71 4 71 5 78 4 0.005 0 0.005-0.5 0.995 0.999 4 -0.5 3 82 89 95 24. 1 3 20 9 10 10 3 18 72 3 77 4 76 5 0.005 0 0.005-0.5 0.999 0.999 -0.5 9 70 71 79 25. 4 - 19 4 4 4 - 17 74 2 70 4 70 4 0.01- 6 0.03-3.0 0.998 19 0.999 1 1.0 86 94 86 1 26. 5 82 17 2 3 3 0.005 3 25 88 10 85 6 104 2 0.005-0.5 0.988 0.994 1 93 87 90 -0.5 27. 5 9 20 5 2 6 0.005 7 19 10 4 116 4 116 5 0.01-0.5 0.999 0.997 8 97 92 98 -0.5 9 28. 1 - 19 2 3 1 1 16 10 1 101 1 101 4 0.005 9 0.01-1.0 0.999 12 0.999 0 -0.5 1 95 89 98 29. 2 84 29 9 15 4 0.005 1 19 84 6 79 6 73 5 0.02-2.0 0.999 0.999 7 73 70 76 -0.5 30. 6 -4 19 4 1 2 0.005 - 18 79 3 81 1 76 4 0.01-0.5 0.999 0.999 92 90 98 -1.0 1 31. 3 -5 19 4 3 5 0.005 2 22 10 7 88 2 90 4 0.03-3.0 0.999 0.999 6 102 93 92 -0.5 1 1 32. 1 - 19 11 12 10 - 24 95 9 78 1 82 4 0.005 0 0.005-0.5 0.999 11 0.999 7 -0.5 4 90 94 106 33. 1 45 17 1 11 3 6 21 94 6 83 2 85 2 0.005 7 0.01-1.0 0.999 0.999 -0.5 6 102 95 103 34. 1 -9 16 10 11 9 - 18 90 5 98 3 89 1 0.005 0 0.005-0.5 0.991 0.999 1 -0.5 5 92 90 102 2 35. 1 - 17 1 1 9 1 23 90 6 90 8 80 2 0.005 9 0.01-1.0 0.999 15 0.999 -0.5 8 90 90 103 36. 1 23 20 3 4 5 1 18 11 6 108 3 115 5 0.005 8 0.02-2.0 0.999 0.999 6 9 -0.5 0 106 96 105 37. 1 -6 19 7 7 5 9 17 98 7 88 2 85 4 0.005 8 0.01-1.0 0.997 0.999 -0.5 5 90 84 95 38. 4 -7 17 2 1 2 0.005 4 18 97 6 85 3 90 2 0.01-1.0 0.999 0.999 7 89 85 89 -0.5 39. 1 41 27 12 10 9 0 27 11 5 119 2 110 2 0.005 5 0.01-1.0 0.999 0.995 8 -0.5 4 103 94 103 40. 3 55 18 9 4 6 0.005 1 20 68 6 78 5 69 3 0.01-1.0 0.999 0.999 2 74 64 68 -0.5 41. 1 9 20 12 12 3 1 16 94 7 80 1 85 1 0.005 9 0.01-1.0 0.999 0.999 4 -0.5 7 98 86 98 42. 1 21 17 8 8 7 2 20 80 6 80 5 90 6 0.005 0 0.01-1.0 0.999 0.997 -0.5 0 86 91 82 43. 1 14 23 14 6 1 2 15 75 6 71 6 82 4 0.005 3 0.05-5.0 0.999 0.999 3 -0.5 7 79 73 72 44. 1 - 22 3 2 2 7 25 10 7 96 13 88 3 0.005 6 0.01-1.0 0.999 10 0.999 2 -0.5 6 88 85 96 45. 4 7 21 12 1 2 0.005 1 14 88 2 89 2 86 2 0.01-1.0 0.999 0.999 1 102 98 99 -0.5 2 46. 5 15 17 6 4 9 0.01- 1 15 85 4 78 3 80 6 0.02-2.0 0.999 0.999 7 90 84 106 1.0 5 47. 1 14 22 12 3 4 4 13 95 7 93 1 82 3 0.005 4 0.01-1.0 0.999 0.999 -0.5 0 105 85 95 48. 2 11 21 2 1 1 0.005 3 15 86 4 91 3 84 2 0.02-2.0 0.999 0.999 96 95 104 -0.5 49. 1 84 23 16 5 9 1 28 95 14 109 8 82 4 0.005 0 0.02-2.0 0.999 0.998 2 -0.5 2 75 66 68 50. 1 0.01-1.0 0.999 18 22 90 13 88 2 93 1 0.005 0.998 1 22 76 13 84 10 102 3 5 -0.5 4 6 51. 3 7 22 3 2 2 0.005 2 13 90 2 88 1 86 3 0.005-0.5 0.999 0.999 5 89 85 89 -0.5 52. 2 21 20 11 1 2 2 15 84 6 95 3 85 1 0.005 1 0.01-1.0 0.999 0.999 -0.5 5 86 84 83 53. 1 -6 20 1 10 8 - 22 94 8 89 10 79 1 0.005 0 0.005-0.5 0.999 0.999 4 -0.5 6 98 91 80 54. 2 8 21 2 1 1 1 14 73 10 90 2 90 2 0.005 0 0.01-1.0 0.999 0.999 2 -0.5 6 87 86 90 55. 2 -1 19 10 9 6 0.005 - 15 68 6 79 4 77 8 0.05-2.5 0.998 0.995 6 63 67 70 -0.5 6 56. 1 -7 23 15 13 16 1 27 11 9 102 5 114 2 0.005 2 0.01-1.0 0.999 0.995 9 -0.5 5 90 88 116 57. 7 -4 21 2 2 2 0.005 5 14 78 4 70 2 74 2 0.01-1.0 0.999 0.999 9 66 61 67 -0.5 58. 1 -8 20 11 3 2 - 15 80 5 90 3 88 1 0.01- 2 0.01-1.0 0.999 0.999 2 1.0 9 94 88 94 59. 1 14 21 4 1 0 3 24 80 5 88 12 90 2 0.005 5 0.01-1.0 0.999 0.995 -0.5 3 89 89 89 60. 1 -7 23 3 5 1 3 15 90 6 84 3 78 4 0.005 7 0.01-1.0 0.999 0.999 -0.5 2 90 88 94 61. 1 - 20 13 1 1 - 13 10 9 115 1 118 1 0.005 9 0.01-1.0 0.999 12 0.999 1 1 -0.5 9 86 85 91 8 62. 8 -6 22 3 1 3 0.005 2 16 80 6 90 4 80 3 0.01-1.0 0.999 0.999 1 91 87 94 -0.5 63. 1 7 17 9 10 2 3 14 90 7 101 2 88 6 0.01- 8 0.01-1.0 0.999 0.998 0 1.0 8 85 80 85 64. 1 -8 21 1 1 1 1 13 93 4 85 1 90 2 0.005 6 0.01-1.0 0.999 0.999 -0.5 8 89 88 91 65. 1 55 20 4 6 6 0.005 5 14 80 8 86 2 71 1 0.01-1.0 0.999 0.998 6 83 94 91 -1.0 9 66. 4 - 21 3 2 2 - 14 60 5 68 2 68 2 0.005 9 0.01-1.0 0.999 30 0.998 2 -0.5 69 65 67 1 67. 4 2 18 14 6 14 0.005 1 14 80 6 83 2 92 7 0.005-0.5 0.999 0.999 83 90 92 -1.0 68. 1 -1 23 5 3 3 1 15 10 2 110 3 106 4 0.005 2 0.01-1.0 0.999 0.998 1 8 -0.5 6 93 86 96 69. 1 4 22 4 3 5 1 13 81 6 90 1 80 3 0.005 3 0.01-1.0 0.999 0.999 5 -0.5 8 97 88 106 70. 8 -7 23 13 2 3 0.005 - 13 80 10 83 1 99 4 0.01-1.0 0.999 0.999 6 90 78 90 -0.5 7 71. 5 45 22 6 4 2 0.005 5 15 80 5 85 3 90 3 0.005-0.5 0.999 0.999 2 98 91 108 -0.5 6 72. 3 5 22 2 2 1 0.005 8 15 80 3 86 3 86 3 0.005-0.5 0.999 0.999 4 89 87 90 -0.5 73. 8 - 23 6 2 3 - 15 10 6 110 3 97 4 0.01- 5 0.02-2.0 0.998 10 0.999 1 3 1.0 98 94 102 6 74. 1 14 20 1 1 1 3 17 70 8 76 5 86 1 0.005 5 0.01-1.0 0.999 0.999 -0.5 5 98 89 90 75. 3 21 22 3 4 4 0.005 1 14 79 10 86 2 99 3 0.01-1.0 0.999 0.998 7 92 101 108 -0.5 76. 2 -6 21 11 4 1 - 14 90 7 85 2 98 2 0.005 8 0.01-1.0 0.999 0.999 4 -0.5 0 89 87 87 77. 1 - 16 6 6 5 1 21 86 10 84 12 102 5 0.005 1 0.01-1.0 0.999 27 0.997 7 -0.5 7 101 95 108 78. 9 94 17 3 4 1 0.005 2 13 80 7 90 1 76 6 0.01-1.0 0.999 0.999 1 98 93 91 -0.5 3 79. 2 14 16 11 1 1 1 13 80 4 75 1 82 5 0.005 0 0.01-1.0 0.999 0.999 -0.5 1 96 89 91 80. 9 0.01-1.0 0.999 6 21 104 4 98 2 99 3 0.005 0.998 3 10 80 12 82 1 102 2 4 -0.5 81. 1 10 20 4 1 2 0.005 2 14 94 5 86 2 86 1 0.01-1.0 0.999 0.999 8 92 84 88 -0.5 82. 2 -9 27 11 16 15 - 13 72 6 73 1 82 6 0.005 0 0.02-2.0 0.999 0.999 8 -0.5 5 116 114 106 83. 1 83 19 10 9 6 1 20 92 8 86 8 102 8 0.01- 0 0.01-1.0 0.999 0.998 1.0 1 110 108 90 84. 4 - 17 5 6 7 0.005 1 13 90 6 89 1 80 6 0.01-1.0 0.995 0.999 3 19 94 84 90 -0.5 4 85. 1 -9 22 9 2 1 1 12 90 4 86 0 82 3 0.005 6 0.01-1.0 0.999 0.999 -0.5 7 91 89 90 86. 1 - 21 1 2 2 1 12 10 13 80 0 76 2 0.005 1 0.01-1.0 0.999 15 0.999 6 1 -0.5 8 98 102 88 87. 1 11 23 4 4 5 1 13 80 4 86 1 88 4 0.005 3 0.01-1.0 0.999 0.999 7 -0.5 1 110 104 98 88. 1 1 16 15 15 9 0 15 10 12 86 3 80 5 0.005 0 0.005-0.5 0.999 0.999 2 -0.5 7 90 106 85 89. 1 15 22 4 6 3 1 19 86 10 104 7 104 3 0.005 5 0.01-1.0 0.999 0.999 -0.5 9 97 95 98 90. 2 96 20 4 4 3 6 15 69 1 69 3 68 1 0.005 0 0.03-3.0 0.998 0.995 5 -0.5 4 61 72 67 91. 1 - 16 12 2 2 - 15 92 5 82 3 90 5 0.005 5 0.01-1.0 0.999 14 0.999 1 -0.5 7 84 90 92 2 92. 2 4 22 1 4 5 0.005 0 17 79 5 78 5 70 1 0.01-0.5 0.997 0.995 5 60 68 62 -0.5 93. 2 -4 21 10 8 7 - 13 65 3 71 1 69 10 0.005 0 0.01-1.0 0.999 0.998 5 -0.5 7 60 69 74 94. 3 0 22 4 2 3 0.005 7 15 10 6 116 3 105 3 0.01-1.0 0.999 0.999 0 103 94 102 -0.5 9 95. 9 7 24 10 1 3 0.005 0 14 68 1 69 2 68 13 0.01-1.0 0.997 0.995 9 63 68 70 -0.5 96. 1 -6 16 6 6 4 1 20 83 7 91 8 78 5 0.005 1 0.01-1.0 0.999 0.999 1 -0.5 9 100 93 95 97. 1 - 22 6 3 2 1 14 98 9 80 2 85 3 0.005 8 0.01-1.0 0.999 14 0.999 0 -0.5 7 99 96 90 98. 2 - 20 2 4 5 1 14 86 7 73 2 75 1 0.01- 0 0.02-2.0 0.999 10 0.999 4 1.0 9 82 89 96 99. 1 13 20 10 2 2 3 14 83 7 84 2 96 1 0.005 6 0.01-1.0 0.999 0.999 -0.5 1 89 86 92 100. 1 -4 21 4 2 2 1 15 88 7 82 3 96 2 0.005 2 0.01-1.0 0.999 0.999 9 -0.5 7 91 93 98 101. 8 - 20 2 2 1 - 19 96 4 89 7 88 1 0.005 7 0.005-0.5 0.998 32 0.995 2 -0.5 90 95 98 5 102. 1 18 22 12 3 3 3 14 86 11 72 2 94 3 0.005 7 0.01-1.0 0.999 0.999 1 -0.5 0 84 90 85 103. 1 -2 21 4 3 3 - 17 77 5 86 5 82 10 0.01- 1 0.05-5.0 0.999 0.997 3 1.0 1 90 98 88 104. 1 -1 22 6 3 3 1 13 80 1 81 1 81 3 0.005 3 0.01-1.0 0.999 0.999 8 -0.5 5 96 91 97 105. 2 30 22 15 4 3 3 16 11 2 117 4 116 3 0.005 1 0.01-1.0 0.999 0.999 3 -0.5 2 88 88 98 106. 1 14 16 3 6 4 0.005 1 13 87 9 79 1 70 5 0.01-1.0 0.998 0.999 7 107 91 105 -1.0 107. 1 - 20 11 2 2 - 17 86 8 96 5 80 1 0.005 5 0.02-2.0 0.999 12 0.999 7 -0.5 2 93 84 91 108. 6 1 23 3 3 2 0.005 0 15 10 11 86 3 82 4 0.005-0.5 0.999 0.999 3 97 93 110 -0.5 3 109. 2 7 21 10 6 6 2 14 86 5 84 2 94 10 0.005 0 0.01-1.0 0.999 0.998 -0.5 0 108 90 100 110. 1 - 16 5 6 3 - 12 71 6 77 0 82 5 0.005 2 0.01-1.0 0.999 15 0.998 1 -0.5 8 105 94 106 9 111. 9 -8 20 15 1 1 - 16 86 5 86 4 95 1 0.01- 8 0.01-1.0 0.999 0.999 1 1.0 92 90 93 8 112. 1 -5 20 2 5 6 1 14 10 2 105 2 106 1 0.005 4 0.02-2.0 0.998 0.999 5 2 -0.5 3 96 87 93 113. 1 - 16 4 4 7 - 13 84 4 91 1 92 5 0.005 1 0.01-1.0 0.999 19 0.997 1 -0.5 0 100 93 106 1 114. 1 16 21 7 3 2 3 16 10 12 90 4 80 2 0.01- 6 0.01-1.0 0.999 0.999 8 4 1.0 5 98 103 92 115. 9 - 20 12 1 1 - 16 96 3 90 4 90 1 0.005 7 0.02-2.0 0.999 13 0.999 1 -0.5 93 94 93 0 116. 1 82 20 8 4 2 7 14 88 2 84 2 86 1 0.005 1 0.01-1.0 0.998 0.999 4 -0.5 2 80 79 73 117. 5 2 21 9 14 8 0.005 0 19 84 1 86 7 85 2 0.005-0.5 0.999 0.999 4 103 96 85 -0.5 118. 1 11 24 13 2 3 7 17 88 3 94 5 94 13 0.005 2 0.01-1.0 0.999 0.999 -0.5 1 101 90 103 119. 1 - 16 3 5 3 - 24 78 11 100 2 90 5 0.01- 7 0.01-1.0 0.999 16 0.999 3 1.0 1 99 98 102 120. 1 7 22 14 15 8 6 17 75 5 65 5 70 3 0.005 5 0.005-0.5 0.998 0.999 4 -0.5 0 96 91 86 121. 9 - 17 7 4 9 - 19 79 6 89 7 80 6 0.005 0 0.01-1.0 0.995 16 0.997 1 -0.5 95 84 90 5 122. 1 0.01-1.0 0.999 - 22 91 4 86 3 94 4 0.005 0.999 1 17 81 1 79 5 80 3 4 13 9 -0.5 2 123. 1 - 23 13 2 3 - 17 84 5 80 5 89 4 0.005 8 0.02-2.0 0.999 38 0.999 1 -0.5 1 91 88 95 5 124. 1 - 16 4 4 6 - 27 72 15 97 15 98 5 0.005 1 0.03-3.0 0.999 12 0.995 1 -0.5 6 114 98 103 5 125. 7 1 22 5 4 2 0.005 4 20 88 5 86 8 96 3 0.01-1.0 0.999 0.999 94 92 90 -1.0 7 126. 2 -7 20 11 3 3 0.005 - 18 90 4 82 6 84 1 0.01-1.0 0.999 0.999 2 87 87 95 -0.5 9 127. 1 11 20 5 6 6 1 23 80 6 90 1 92 9 0.005 3 0.01-1.0 0.996 0.990 6 -0.5 0 104 96 100 128. 9 -9 20 10 12 1 0.005 - 17 10 5 111 5 114 1 0.01-1.0 0.999 0.997 6 92 94 84 -0.5 1 5 129. 1 9 17 7 2 4 1 24 94 4 85 2 90 6 0.005 4 0.01-1.0 0.999 0.998 -0.5 8 103 84 102 130. 6 -5 22 9 10 7 0.005 1 22 74 3 75 1 80 3 0.005-0.5 0.999 0.999 6 93 106 90 -0.5 131. 2 - 20 3 3 1 0.005 - 19 76 3 74 7 80 1 0.01-1.0 0.999 0.999 1 14 94 88 95 -0.5 3 132. 1 8 20 0 2 3 4 20 79 9 79 8 94 1 0.01- 4 0.01-1.0 0.999 0.998 1.0 4 94 94 110 133. 1 - 21 6 4 2 1 28 96 5 86 8 94 2 0.005 2 0.01-1.0 0.999 12 0.999 0 -0.5 2 97 93 96 134. 4 67 20 2 1 3 0.005 2 20 88 2 90 8 91 1 0.01-1.0 0.999 0.999 2 92 86 85 -0.5 6 135. 6 12 18 1 1 3 0.005 0 21 92 1 90 9 90 3 0.005-0.5 0.999 0.999 4 95 106 100 -0.5 136. 3 15 28 8 10 10 0.01- 6 15 87 1 84 3 85 13 0.01-1.0 0.999 0.998 8 91 90 106 1.0 137. 8 6 30 14 10 12 0.005 3 24 86 4 89 2 94 14 0.02-2.0 0.999 0.999 9 104 96 102 -0.5 138. 6 0.01-1.0 0.999 - 17 91 1 84 2 90 5 0.005 0.996 - 25 80 10 100 3 86 2 1 14 -0.5 6 139. 7 - 26 7 5 12 - 25 80 9 89 5 70 11 0.005 0 0.01-1.0 0.999 13 0.999 1 -0.5 97 94 112 5 140. 1 21 19 10 3 5 4 24 84 5 84 8 76 4 0.005 4 0.005-0.5 0.999 0.998 8 -0.5 9 95 97 96 141. 1 - 22 15 3 7 - 18 80 5 71 2 78 7 0.005 4 0.005-0.5 0.995 20 0.999 2 -0.5 5 96 97 96 0 142. 1 -9 19 12 3 3 9 24 86 0 86 8 86 4 0.005 4 0.01-1.0 0.999 0.999 -0.5 6 98 92 98 143. 7 16 17 11 2 1 0.005 2 24 89 6 90 8 80 2 0.01-1.0 0.999 0.996 1 91 87 96 -0.5 8 144. 2 -5 16 3 1 4 4 20 87 4 94 4 90 1 0.005 1 0.01-1.0 0.999 0.995 -0.5 0 98 91 94 145. 1 - 28 9 14 18 - 18 92 6 80 2 86 13 0.005 1 0.03-1.5 0.998 12 0.999 1 -1.0 98 112 110 2 146. 6 13 21 16 4 5 0.005 1 20 92 3 90 4 86 6 0.01-1.0 0.999 0.999 5 106 96 108 -0.5 5 147. 1 - 25 8 5 7 1 20 90 2 88 4 87 10 0.005 8 0.01-1.0 0.999 29 0.999 8 -0.5 9 93 90 82 148. 1 - 22 6 4 5 - 19 89 8 73 3 83 7 0.005 2 0.02-2.0 0.999 10 0.998 9 -0.5 4 96 89 92 149. 8 68 25 14 10 7 0.01- 2 22 88 5 82 6 91 10 0.01-1.0 0.995 0.995 0 106 91 100 1.0 3 150. 1 - 20 4 2 1 2 17 84 4 86 1 79 4 0.005 7 0.01-1.0 0.999 12 0.999 -0.5 8 88 89 88 151. 1 - 18 2 8 11 - 18 83 5 87 2 92 9 0.005 5 0.005-0.5 0.999 10 0.997 1 -0.5 1 96 90 104 9 152. 3 34 18 1 2 2 0.005 5 20 77 8 85 4 93 2 0.01-1.0 0.997 0.998 1 96 90 94 -0.5 153. 2 -6 20 15 25 17 - 17 90 4 89 1 97 11 0.005 1 0.01-1.0 0.999 0.999 1 -0.5 1 86 81 100 0 154. 9 26 17 2 3 10 0.005 7 16 80 4 81 0 88 1 0.01-1.0 0.999 0.999 2 91 85 98 -0.5 155. 1 -9 18 12 13 3 - 17 91 1 92 1 90 2 0.005 9 0.02-2.0 0.999 0.999 2 -0.5 4 90 94 84 156. 2 - 21 10 1 7 0.005 0 22 78 5 71 6 80 5 0.03-3.0 0.998 0.999 4 25 72 75 83 -0.5 157. 1 32 20 10 1 5 - 22 88 3 89 6 93 4 0.01- 7 0.05-5.0 0.999 0.999 2 1.0 5 104 96 96 5 158. 5 9 19 3 3 3 0.005 1 27 95 5 88 1 85 3 0.01-0.5 0.999 0.999 6 104 88 103 -0.5 1 159. 6 - 18 11 4 2 - 27 76 3 72 1 78 2 0.005 8 0.01-1.0 0.999 25 0.998 1 -0.5 98 98 101 6 160. 2 - 16 11 7 10 - 27 80 4 88 11 84 7 0.005 1 0.01-1.0 1.000 12 0.998 9 -0.5 6 86 78 84 161. 1 - 21 10 12 13 - 28 99 12 83 2 75 12 0.005 1 0.02-2.0 0.995 39 0.998 2 -0.5 5 80 78 72 5 162. 2 - 19 3 3 2 - 27 90 5 82 1 81 3 0.005 0 0.01-1.0 0.999 13 0.997 1 -0.5 92 84 95 8 163. 1 - 16 6 6 6 - 26 90 5 80 1 89 7 0.005 6 0.01-1.0 0.999 15 0.998 1 -0.5 4 104 94 102 4 164. 1 - 20 3 6 5 0.01- - 22 86 4 88 6 93 4 0.01-1.0 0.999 0.998 39 97 96 102 1.0 1 165. 2 5 20 5 12 7 9 23 83 6 95 7 89 4 0.005 0 0.01-1.0 0.999 0.998 -0.5 3 104 97 108 166. 1 12 20 14 4 4 0.005 3 18 92 3 93 2 88 4 0.01-1.0 0.999 0.998 9 104 94 108 -0.5 5 167. 6 -2 19 4 4 5 0.005 1 28 80 10 89 2 100 3 0.01-1.0 0.999 0.999 7 90 93 84 -0.5 2 168. 2 - 18 1 2 2 0.01- - 17 70 3 73 1 76 2 0.01-1.0 0.999 0.999 8 14 60 66 68 1.0 3 169. 8 - 22 12 5 5 0.005 - 23 75 7 89 7 82 6 0.02-2.0 0.999 0.999 3 10 103 96 106 -0.5 1 170. 6 80 16 6 3 4 0.005 5 25 76 5 80 9 85 7 0.01-1.0 0.999 0.999 0 106 95 89 -0.5 7 171. 2 - 26 4 2 1 - 20 89 2 86 4 90 17 0.01- 9 0.02-2.0 0.999 40 0.999 1 1.0 87 89 82 0 172. 1 13 17 3 1 2 0.005 9 17 76 5 80 1 70 1 0.01-1.0 0.999 0.999 3 95 93 99 -1.0 173. 1 - 16 12 17 8 - 22 79 3 80 6 84 7 0.005 3 0.01-1.0 0.999 21 0.997 1 -0.5 6 94 89 100 8 174. 1 - 18 2 2 10 - 17 76 1 71 1 80 9 0.005 2 0.02-1.0 0.997 35 0.997 2 -1.0 86 96 82 5 175. 8 -7 16 5 3 3 0.005 - 26 85 4 92 10 91 2 0.01-1.0 0.999 0.997 4 91 86 93 -0.5 5 176. 7 - 16 13 2 1 0.005 - 21 96 5 87 5 97 2 0.02-2.0 0.999 0.999 3 13 88 85 94 -0.5 3 177. 1 -5 18 6 4 7 2 17 90 1 88 1 89 4 0.005 3 0.01-1.0 0.998 0.998 -0.5 2 89 86 96 178. 7 - 18 4 5 7 0.005 1 20 93 9 87 4 76 4 0.02-2.0 0.999 0.999 5 27 93 88 84 -0.5 8 179. 1 -8 16 2 2 3 - 21 85 8 70 5 77 2 0.005 9 0.02-2.0 0.999 0.999 4 -0.5 5 94 108 100 180. 7 - 20 14 5 6 0.005 - 21 80 2 84 5 80 6 0.01-1.0 0.999 0.999 7 20 99 92 96 -0.5 9 181. 2 11 17 1 2 2 6 19 92 3 86 3 87 3 0.005 0 0.01-1.0 0.999 0.999 -0.5 2 110 94 94 182. 2 63 17 4 5 4 1 18 90 2 94 2 91 1 0.005 1 0.01-1.0 0.999 0.996 -0.5 4 92 93 90 183. 9 19 22 9 9 6 0.005 1 22 88 6 86 6 98 8 0.01-0.5 0.999 0.997 102 94 102 -1.0 184. 9 4 25 13 2 9 0.005 5 19 85 4 78 3 86 11 0.01-1.0 0.999 0.997 5 90 99 105 -0.5 185. 1 - 18 5 3 5 2 17 99 8 92 1 84 4 0.005 6 0.01-1.0 0.999 45 0.995 2 -0.5 3 98 90 102 186. 1 - 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17 2 1 1 - 18 81 3 80 2 76 1 0.005 3 0.01-1.0 0.999 13 0.999 1 -0.5 92 90 94 0 200. 1 -9 19 7 5 4 - 21 88 2 92 5 90 5 0.005 6 0.01-1.0 0.999 0.999 1 -0.5 9 94 90 98 201. 7 - 16 12 11 2 - 18 82 4 82 2 89 2 0.005 8 0.01-1.0 0.999 14 0.999 1 -0.5 86 92 86 8 202. 3 12 21 10 7 7 0.01- 5 24 89 8 76 4 91 7 0.01-1.0 0.999 0.999 9 102 91 96 1.0 203. 4 5 17 5 3 3 0.005 1 26 85 4 78 6 86 3 0.03-3.0 0.999 0.999 0 101 102 94 -0.5 204. 1 10 16 11 1 2 0.005 1 25 96 5 85 9 89 2 0.02-1.0 0.999 0.999 5 97 93 94 -1.0 7 205. 1 -9 16 11 4 1 3 27 10 10 84 11 85 2 0.005 9 0.02-2.0 0.999 0.998 1 -0.5 0 91 89 96 206. 6 53 19 5 3 5 0.01- 0 20 75 3 70 4 75 5 0.02-2.0 0.999 0.999 9 101 95 108 1.0 207. 1 - 23 17 8 9 - 24 83 2 86 8 84 9 0.005 8 0.03-3.0 0.999 28 0.996 1 -0.5 2 111 98 98 9 208. 1 29 18 9 7 14 1 22 70 4 76 6 77 4 0.01- 9 0.01-1.0 0.999 0.999 1.0 3 105 115 109 209. 5 -1 18 12 1 1 - 27 91 5 89 11 81 4 0.005 5 0.01-1.0 0.999 0.995 1 -0.5 91 90 92 0 210. 4 20 18 7 3 3 0.005 1 27 12 4 116 2 112 4 0.02-2.0 0.999 0.999 5 96 87 88 -0.5 0 211. 1 7 20 17 5 7 0 18 91 4 84 2 88 6 0.005 1 0.02-2.0 0.999 0.999 -0.5 4 105 93 93 212. 1 -9 18 4 2 5 0.005 - 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