FT/GN/65C/00/20.07.16
SRI VENKATESWARA COLLEGE OF ENGINEERING
COURSE DELIVERY PLAN - THEORY Page 1 of 6
Department of Chemical Engineering LP: Sub Code
B.E/B.Tech/M.E/M.Tech : M. Tech Regulation: 2018 CL18102 PG Specialisation : Chemical Engineering Rev. No: 0 Sub. Code / Sub. Name : CL18102/Advanced Separation processes Date: 06-01-2021 Unit : I Unit Syllabus: BASICS OF SEPARATION PROCESS: Review of conventional processes, recent advances in separation techniques based on size, surface properties, ionic properties and other special characteristics of substances. Process concept, theory and equipment used in cross flow filtration, cross flow electrofiltration, dual functional filter, surface based solid-liquid separations involving a second liquid.
Objective: To review present practices of separation processes and provide principles and technical concepts of basics of separation processes based on size, surface and ionic properties.
Session Teaching Topics to be covered Ref No:PP No * Aids Review of conventional separation processes ex. Adsorption and PPT/BB/ON 1 stripping, Distillation, Extraction, Crystallization & Evaporation, 2:140-160 LINE Drying, Filtration, Settling etc Separation Techniques based on size like membrane separation PPT/BB/ON 2 4:61-76 processes such as micro, ultra and nano filters and reverse osmosis LINE Separation techniques based on surface properties, Physical PPT/BB/ON 3 6:30-36 adsorption & Chemical adsorption, Chromatography, LINE Separation techniques based on ionic properties, Mechanism of ion- PPT/BB/ON 4 1:631-632 exchange process, Types of resins, Ion exchange chromatography LINE PPT/BB/ON 5 Process concept, Unit operation, Separation Mechanisms 2:40-50 LINE Cross Flow Filtration, Normal Flow Filtration and Cross Flow PPT/BB/ON 6 8:239-240 Filtration differences, Cross Flow Filtration modules LINE Cross Flow Filtration modules, Theory, Alternate electrode PPT/BB/ON 7 8:241-250 configurations LINE PPT/BB/ON 8 Surface based solid – liquid separations involving a second liquid 1:20.28-29 LINE PPT/BB/ON 9 Problems based on basic separation processes 1:Notes LINE Content beyond syllabus covered (if any): Reverse Osmosis systems for water treatment in India
* Session duration: 50 minutes
FT/GN/65C/00/20.07.16
SRI VENKATESWARA COLLEGE OF ENGINEERING
COURSE DELIVERY PLAN - THEORY Page 2 of 6
Sub. Code / Sub. Name: CL18102/Advanced Separation processes Unit : III
Unit Syllabus: Bubble and Foam Fractionation: Nature of bubbles and foams, stability of foams, foam fractionation techniques, batch, continuous, single stage and multistage columns, Types of equipment and commercial processes.
Objective: to understand bubble and foam fractionation surfactant types and their use for solving problems in industry and environment
Session Teaching Topics to be covered Ref No:PP No * Aids PPT/BB/ON 20 Definition of bubble and foam fractionation 6:2-27 LINE PPT/BB/ON 21 Nature of Bubbles and foams 1:16.8-9 LINE PPT/BB/ON 22 Foam fractionation techniques 1:16.8-9 LINE
PPT/BB/ON 23 Adsorptive bubble separation techniques 6:48-52 LINE
PPT/BB/ON 24 Batch and column studies 2:178-180 LINE
PPT/BB/ON 25 Single stage and multistage foam fractionation columns Notes LINE
PPT/BB/ON 26 Types of equipment and commercial processes Notes LINE
PPT/BB/ON 27 Recent advances In bubble and foam fractionation processes Notes LINE
Process economics of bubble and foam fractionation processes PPT/BB/ON 28 Notes LINE PPT/BB/ON 29 Notes Revision LINE Content beyond syllabus covered (if any): Pilot experiments in batch and column studies.
* Session duration: 50 minutes
FT/GN/65C/00/20.07.16
SRI VENKATESWARA COLLEGE OF ENGINEERING
COURSE DELIVERY PLAN - THEORY Page 3 of 6
Sub. Code / Sub. Name: CL18102/Advanced Separation processes Unit : II
Unit Syllabus: MEMBRANE SEPARATIONS: Types and choice of membranes, plate and frame, tubular, spiral wound and hollow fibre membrane reactors and their relative merits, commercial, pilot plant and laboratory membrane pemeators involving dialysis, reverse osmosis, nanofiltration, ultrafiltration, microfiltration and Donnan dialysis, economics of membrane operations, ceramic membranes. Objective: Comprehensive understanding of different membrane processes and application of these processes to solve separation problems in industry and environmental issues.
Session Teaching Topics to be covered Ref No:PP No * Aids Definition of a membrane, Types of Membranes, Driving Forces, Properties PPT/BB/ON 10 4:17-31 of membranes LINE Types of Membranes, Symmetric membranes, Asymmetric membranes, PPT/BB/ON 11 8:15-48 Characteristics of the membranes, Membrane characterization LINE Membrane Module Configurations, Spiral-wound configuration, Tubular PPT/BB/ON 12 8:133-139 configuration, Capillary/hollow fiber configuration LINE Working philosophy of pressure driven membrane process, RO, NF, UF PPT/BB/ON 13 4:61-74 and micro filtration, Permeation rate, merits of Membranes LINE Desalination, s, Desalination by RO, Flow-sheet of sea water desalination, , PPT/BB/ON 14 1 Notes: Desalination Plants. LINE PPT/BB/ON 15 Donnan Dialysis, principle, 4:86-91 LINE PPT/BB/ON 16 Economics of membrane operations 1: Notes LINE PPT/BB/ON 17 Ceramic Membranes 8:5 LINE PPT/BB/ON 18 Membrane bio reactors, Types of MBRs, Application of MBRs 4:187-194 LINE PPT/BB/ON 19 Revision 1: Notes LINE Content beyond syllabus covered (if any): Types of desalination plants in India
* Session duration: 50 minutes
FT/GN/65C/00/20.07.16
SRI VENKATESWARA COLLEGE OF ENGINEERING
COURSE DELIVERY PLAN - THEORY Page 4 of 6
Sub. Code / Sub. Name: CL18102/Advanced Separation processes Unit : III
Unit Syllabus: Bubble and Foam Fractionation: Nature of bubbles and foams, stability of foams, foam fractionation techniques, batch, continuous, single stage and multistage columns, Types of equipment and commercial processes.
Objective: to understand bubble and foam fractionation surfactant types and their use for solving problems in industry and environment
Session Teaching Topics to be covered Ref No:PP No * Aids PPT/BB/ON 20 Definition of bubble and foam fractionation 6:2-27 LINE PPT/BB/ON 21 Nature of Bubbles and foams 1:16.8-9 LINE PPT/BB/ON 22 Foam fractionation techniques 1:16.8-9 LINE
PPT/BB/ON 23 Adsorptive bubble separation techniques 6:48-52 LINE
PPT/BB/ON 24 Batch and column studies 2:178-180 LINE
PPT/BB/ON 25 Single stage and multistage foam fractionation columns Notes LINE
PPT/BB/ON 26 Types of equipment and commercial processes Notes LINE
PPT/BB/ON 27 Recent advances In bubble and foam fractionation processes Notes LINE
Process economics of bubble and foam fractionation processes PPT/BB/ON 28 Notes LINE PPT/BB/ON 29 Notes Revision LINE Content beyond syllabus covered (if any): Pilot experiments in batch and column studies.
* Session duration: 50 minutes
FT/GN/65C/00/20.07.16
SRI VENKATESWARA COLLEGE OF ENGINEERING
COURSE DELIVERY PLAN - THEORY Page 5 of 6
Sub. Code / Sub. Name: CL18102/Advanced Separation processes Unit : IV
Unit Syllabus: SPECIAL PROCESSES Liquid membrane separation, super-critical extraction, adsorptive separation pressure, vacuum and thermal swing, pre vaporation, separation of isotopes, Commercial processes, Industrial applications
Objective: Gain the knowledge of separations based on ionic charge of the species and separation of them in critical separations.
Session Teaching Topics to be covered Ref No:PP No * Aids PPT/BB/ON 30 Liquid membrane separation 2:124-127 LINE PPT/BB/ON 31 Super critical extraction Notes LINE PPT/BB/ON 32 Adsorptive separation pressure 1:20.19-20.20 LINE PPT/BB/ON 33 Vacuum and thermal swing 20.23-20.24: LINE PPT/BB/ON 34 Pervaporation and permeation Notes LINE PPT/BB/ON 35 Separation of isotopes 4:153-161 LINE PPT/BB/ON 36 Nano-separation Notes LINE PPT/BB/ON 37 4:163-167 Commercial processes and industrial applications LINE PPT/BB/ON 38 Revision Notes LINE Content beyond syllabus covered (if any): Practical application of special processes
* Session duration: 50 minutes
FT/GN/65C/00/20.07.16
SRI VENKATESWARA COLLEGE OF ENGINEERING
COURSE DELIVERY PLAN - THEORY Page 6 of 6
Sub. Code / Sub. Name: CL18102/Advanced Separation processes Unit : V
Unit Syllabus: Chromatographic Methods of Separation: Gel, Solvent, Ion and High performance liquid chromatography. Industrial applications and R&D Effluent treatment methods Objective: To learn advanced rare separation processes and their applications in industry and environment
Session Teaching Topics to be covered No:PP No * Aids PPT/BB/ON 39 Gel separation 1: Notes LINE PPT/BB/ON 40 Solvent extraction 4:147-150 LINE 1:20.5 – PPT/BB/ON 41 Gas chromatography 20.6 LINE PPT/BB/ON 42 Ion chromatography 1: Notes LINE 1:20.14- PPT/BB/ON 43 high performance liquid chromatography 20.17 LINE PPT/BB/ON 44 Industrial applications and R&D Notes LINE PPT/BB/ON 45 Effluent treatment techniques 1: Notes LINE Content beyond syllabus covered (if any):