Manufacturing of Synthetic Resins with Formulae & Processes

Manufacturing of Synthetic Resins with Formulae & Processes (allyl resins, alkyd resins, electro deposition primers, zinc rich coatings, alginate, carboxymethyl cellulose, carrageenan, guar gum, polyethylene glycol, alginate, polyvinyl pyrrolidone, silicones resins) Introduction

Synthetic resin is typically manufactured using a chemical polymerization process. This process then results in the creation of polymers that are more stable and homogeneous than naturally occurring resin. Since they are more stable and are cheaper, various forms of synthetic resin are used in a variety of products such as plastics, paints, varnishes, and textiles. There are various kinds of synthetic resins; silicones resins, polyvinyl pyrrolidone, gum arabic, epoxy resins, guar gum, carrageenan, carboxymethyl cellulose, etc. Resins are polymeric compound which are available in nature and are also manufactured by synthetic routes. Some resins are also manufactured by partial modification of natural precursor polymer by chemical. www.entrepreneurindia.co Silicones are unique among the commercially important polymers both in chemistry and in variety of industrial applications. Silicones can be applied as high temperature insulating varnishes, impregnates to be used with glass, asbestos, mica products and encapsulating agents for electrical components. Water borne dispersions or emulsions, for example emulsions of vinyl or acrylic copolymers are popular in decorative coatings. The applications of synthetic resins are seen in some important industries like paint industry, adhesive industry, the textile industry, paper, paint, agricultural industry, petroleum industry etc. As it can be seen that there is an enormous scope of application of resins hence it is one of the major field to venture. www.entrepreneurindia.co Some of the fundamentals of the book are electrodepositable pigmented coating compositions based on alkyd resins, phosphorus containing allyl resins, vapour permeation cure technology, characterization of water soluble anodic electrodepositive pigmented coating compositions, protection of concrete substrates, zinc rich coatings, electro deposition primers, developments in thermosetting powder coatings, application of powder coatings, polyethylene glycol, petroleum recovery and processing, industries using polyethylene glycols, silicones resins, preparation & formulation of silicone resin based coatings, pigments and dyes etc. Resin is a thermosetting synthetic polymer having properties such as adhesive strength, luster, and hardness. www.entrepreneurindia.co Epoxy resins are available in the form of liquid as well as high viscosity solid. Epoxy resins are segmented on the basis of applications such as follow-paints & coatings, electrical & electronics, wind energy, construction, and composites. During 2009–2013, consumption of epoxy resins for coatings increased at an average annual rate of 8.3% and for electrical and electronics applications at 6.8%. Epoxy resins for composite applications increased at an average rate of 8.1% per year In 2013, the largest end use for epoxy resins was coating applications, which accounted for 43% of total consumption, followed by electrical and electronics applications, at 35%. The resin market accounted for USD 7.54 Billion in 2015 and is expected to reach USD 11.22 Billion by 2021, growing at a CAGR www.entrepreneurindia.co of around 6.9% between 2016 and 2021.In INDIA, epoxy resins consumption will grow at an average annual rate of 4.9% for 2013–2018. Epoxy resin consumption for composites in the United States is forecast to grow at an average annual rate of nearly 10% during 2013–2018. Synthetic Resins are used by lot of industries. Yet, little emphasis has been placed on the comparative value on functionality of polymeric material as a class. These resins have been classified in separate categories, usually in terms of their Chemistry, sources or end uses. The present book contains formulae, processes and other valuable details for various synthetic resins. This is very useful book for those concerned with development, consultants, research scholars, new entrepreneurs existing units, institutional libraries etc. www.entrepreneurindia.co Tabl e of Cont ent s 1. PHOSPHORUS CONTAINING ALLYL RESINS

Properties of Monomers Polymerization Applications

2 . ELECTRODEPOSITABLE PIGMENTED COATING COMPOSITIONS BASED ON ALKYD RESINS

Introduction Experimental Materials Synthesis of water soluble alkyd resin from phthalic anhydride and maleic anhydride (A1). www.entrepreneurindia.co Synthesis of water soluble alkyd resin from phthalic anhydride and trimellitic anhydride (A2). Synthesis of water soluble alkyd resin from phthalic anhydride and maleopimaric acid (A3). Synthesis of water soluble alkyd resin from maleopimaric acid (A4). Synthesis of water soluble methylated melamine formaldehyde resin. Preparation of water soluble anodic electrodepositive pigmented coating compositions. www.entrepreneurindia.co Testing and evaluation of anodic electrodepositive pigmented coating compositions Results and Discussions Solvent (MTO) Resistance Protection Against Corrosion

3. VAPOUR PERMEATION CURE TECHNOLOGY Introduction Vapour Permeation Cure (VPC) Primary Advantages of VPC Coating Disadvantages Limitations Vapour Injection Cure (VIC) Process Chemical Composition Reaction and Mechanism

www.entrepreneurindia.co Advantages of VIC Conclusion

4. PROTECTION OF CONCRETE SUBSTRATES Differences Between Concrete and Metallic Substrates Constructions Influence Coatings Used on Concrete Organic coatings Thin film Modified Epoxies Furans Chlorinated Rubbers Waterborne Coatings Vinyl Esters Other Coatings

www.entrepreneurindia.co Organic Coatings Thick Film Elastomeric Coatings Polyurethane Coatings Synthetic Rubber (Elastomers) Resin Rich System Polymer Concretes Plastic Liners Brick or Tile and Mortar Systems Machinery Setting Grouts Inorganic Coatings New Versus Aged or Deteriorated Substrates Quality Assurance Conclusion 5. ZINC RICH COATINGS Inhibitive Primers www.entrepreneurindia.co Organic Zinc Rich Coatings Inorganic Zinc Rich Coatings Surface Preparation White Metal Blasting Galvanising Galvanising and Zinc Rich Coating Comparison Beach Front Exposure Tidal Exposure 5% Salt Spray Test Inorganic Zinc Rich Coating Advantages and Limitations Application of Inorganic Zinc Rich Coatings Cost Aspects 6. ELECTRO DEPOSITION PRIMERS Electrodeposition Primers Mechanism of Electrodeposition Electro osmosis www.entrepreneurindia.co Advantages of Electrodeposition Types of Electrodeposition Primers Shift to Cathodic E.D. Primer Cathodic Electrodeposition Paint Comparison of AED and CED Properties of Dry Film Latest Development in C.E.D. Comparative Features of Different Types of CED Plant Design and Process Control Trends in Top Coats Up gradation of Appearance & Performance of Top Coats Solid Colors Metallic Colors Developments in Top Coat Application Developments in Thermosetting Powder Coatings www.entrepreneurindia.co Powder Manufacture Types of Powder Powder Coatings Method of Application Electrostatic Spray Corona Charging Faraday Cage Back Ionization Electrostatic Spray Tribo Charging Advantages of Powder Coatings Dis Advantages of Powder Economic Advantages of Powder Coatings Application of Powder Coatings General Metal Coatings Industrial Machinery Conclusion

www.entrepreneurindia.co 7. WATERBORNE DISPERSIONS Formulating Principles Pigments Additives Binders Acrylics/Vinyls/Vinyl Acrylic Emulsions Polyurethane Dispersions Cross Linking Epoxy Dispersions Miscellaneous Systems Conclusion

8. ALGINATE Chemical Structure Chemical Derivatives Manufacture www.entrepreneurindia.co Physical Properties Powdered Alginates Solution Properties Rheological Properties Commercial Uses Food Applications Industrial Applications Formulations Stabilizing Frozen Foods Fruit pie Filling Frozen Gel Frozen Fruit Cream Sauce Barbecue Sauce Frozen Shortcake Berry Filling www.entrepreneurindia.co Frozen Gel Frozen Fruit Cream Sauce Barbecue Sauce Frozen Shortcake Berry Filling Tomato Sauce (Pizza and Spaghetti) Macaroni and Cheese Chopsuey Food Gels Dessert Gel Cold Water Gel Cold Milk Gel Instant Chiffon Pie Filling Instant Cheese Cake Mix Instant Limitation Bakery Jelly Banana Gel Base www.entrepreneurindia.co Meringue Powder with Dried Egg Whites Dessert Souffles Vanilla Souffle Chocolate Souffle Lemon Souffle Dressings Fabricated fruit Pie fillings Cooked Fillings Cold mix Fillings Industrial Applications Corrugating Adhesives Single Starch System Two Starch System Fiber Reactive dyes www.entrepreneurindia.co Pad Dyeing Laboratory Techniques Viscosity Measurement Moisture Determination Powder Color Determination Alginates in Mixtures (Detection) Alginates in Mixtures (Determination) Spectrophotometric

9. CARBOXYMETHYL CELLULOSE Chemical Nature Physical Properties Equilibrium Moisture Content Molecular Weights Solubility Film Properties www.entrepreneurindia.co Manufacture Biological Properties Toxicological Properties Six month Oral Toxicity One year Studies Chronic Oral Toxicity Reproduction Gastrointestinal Absorption Clinical Study Skin Irritation and Sensitization Getting Information Rheology Storage and Handling Packaging In Plant Handling Bulk Handling www.entrepreneurindia.co Bag Handling and Storage Shipping Applications Detergents Petroleum Paper Textiles BOD and Desizing Wastes Coatings Cosmetics and Pharmaceuticals Miscellaneous Applications Specialties Future Developments World Production

www.entrepreneurindia.co 1 0. CARRAGEENAN Chemical Nature Structure Molecular Weight Reactivities Physical Properties Appearance Particle Size Density Solubility's Manufacture Biological/Toxicological Properties Gastrointestinal Ulceration Teratogenicity Carcinogenicity www.entrepreneurindia.co Rheological Properties Gelation Milk Gels Additives/Extenders Handling Applications By Result By End Product By Industry By Process Application Procedures Dispersion Stability Specialties Future Developments Commercial Uses: Compounding and Formulating www.entrepreneurindia.co Milk Applications Uses in Dry Mixes Uses in Manufactured Products Water Applications Uses in Dry Mixes Uses in Manufactured Products Nonfood Applications Pharmaceuticals and Toilet Goods Other Applications Commercial Uses: Processing Aids Beverage Clarification Abrasive Suspensions Ceramic Glazes and Core Washes Industries Using Carrageenans Food Dairy www.entrepreneurindia.co Dairy Substitutes Packaged Desserts Other Food Uses Pharmaceuticals and Toilet Goods Metal Fabrication Ceramics Coatings Agriculture Household Products Formulations Chocolate Milk Canned Water Dessert Gel Air Treatment Gel Toothpaste Milk Puddings Creamy Type (Cold Set) www.entrepreneurindia.co Cooked Custard Type (Dessert and pie filling) Cooked Custard or Flan Antacid Gel Laboratory Techniques Water Viscosity Measurement Water Gel Strength Measurement Milk Gel Strength measurement

11. GUAR GUM Manufacture Seed Structure Purification Grades Chemical and Physical Properties Structure Solubility in Water www.entrepreneurindia.co Rheology Viscosity Shear Response Handling Dry Storage Solution Preparation Applications Oil and Gas Explosives Textile Food Ice Cream Canned Pet Food Cheese Sauces and Salad Dressings Paper www.entrepreneurindia.co Mining Commercial Applications: Compounding and Formulating Food Explosives Commercial Uses: Processing Aids Oil and Gas Textile Carpets Paper Kraft Papers Kraft Liner board Recycled Liner board Corrugating Medium Boxboard Offset News Stock White Papers www.entrepreneurindia.co Mining Industries Using Guar Gum Oil and Gas Explosives Food Paper Textile Mining Formulations

12. GUM ARABIC Chemical Nature Physical Properties Manufacture Biological/Toxicological Properties Rheological Properties www.entrepreneurindia.co Additives/ Extenders Additives Extenders Handling Applications Emulsification Colloid Stabilization Encapsulation Suspension Application Procedures Compatibility Commercial Uses Food Applications Confectioneries Dairy Products www.entrepreneurindia.co Bakery Products Flavor Fixation Flavor Emulsification Beverages Pharmaceuticals Suspending Agent Demulcent Agent Emulsification Antiseptic Preparations Miscellaneous Applications Medicines Cosmetics Adhesives Paints Inks www.entrepreneurindia.co Record Ink Soluble Inks Watercolor Inks Quick Drying Inks Fabric and Laundry Marking Inks Pigmented Inks Emulsion or Typographic Inks Hectographic Inks Electrically Conductive Inks Lithography Textiles Miscellaneous Uses Industries Using Gum Arabic Food Industry Pharmaceutical Industry www.entrepreneurindia.co Other Industries Formulations Confectioneries Dietetic or Sugarless Candies Marshmallows Food Emulsions Pickle Oil Emulsion Pickle Juice Beverages Stabilized Fruit Drink Dry Mix Imitation Orange Drink Beverage Stabilizers Nut Coating Inks Gloss Finish Inks www.entrepreneurindia.co Wood Grain Inks Laboratory Techniques 30% Viscosity Method Insoluble Residue Sediment and Color Peroxidase Content

1 3. HYDROXY ETHYL CELLULOSE Chemical Nature Stability Physical Properties Solubility in water Solubility in Organic Solvents Dissolving Methods Viscosity Properties Compatibilities www.entrepreneurindia.co Manufacture Biological/Toxicological Properties Rheological Properties of Solutions Additives/Extenders Handling Applications Application Procedures Specialties Future Developments Commercial Uses: Compounding and Formulating Protective Colloid in Latex Thickener for Latex Compositions Latex Paints Color Coats for Paper Textile Binders and Adhesives www.entrepreneurindia.co Building Specialties Cosmetics and Pharmaceuticals Paper Sizes and Coatings Carpet and Textile Dye Pastes Special Applications Commercial Uses: Processing Aids Crude Oil Drilling and Recovery Electroplating and Electrowinning Miscellaneous Binders Other Specialty Uses Industries Using Hydroxyethylcellulose Adhesives Agricultural Products Building Products Cosmetics Oil and Gas Extraction www.entrepreneurindia.co Paints and Coatings Paper and Allied Products Synthetic Resins Textile Mill Products Formulations Copolymer Latex Latex Interior Flat Wall Paint Textile Printing Oil Well Work over Fluid Roll on Antiperspirant Liquid Shampoo

1 4. HYDROXY PROPYL CELLULOSE Chemical Nature Stability Chemical Stability www.entrepreneurindia.co Biological Stability Insolubilization Physical Properties Moisture Content Solutions Rheology Organic Solutions Hot Melts and Waxes Compatibility Film Properties Thermo plasticity Manufacture Toxicological Properties Additives Preservatives Defoamers www.entrepreneurindia.co Plasticizers Handling Applications Application Procedures Water Temperature Compatibility with Salts Molding Powder Preparation Specialties Commercial Uses: Compounding and Formulating Commercial Uses: Processing Aids Industries Using Hydroxypropyl Cellulose Formulations Cosmetics Antiperspirant (Roll On) Hair Grooming Aid Shampoo (Gel) www.entrepreneurindia.co Paint Removers Nonflammable Solvent Type Remover Acid Type Remover Pharmaceuticals Thermoplastics Injection Molding Formulation (Unfilled) Laboratory Techniques

1 5. POLYETHYLENE GLYCOL Chemical Nature Physical Properties Viscosity Solubility in Water Solubility in Organic Solvents Solvency and Compatibility Hygroscopicity www.entrepreneurindia.co Surface Tension Volatility Thermal Stability Biological/Toxicological Properties Manufacture Handling Applications Functions End Products Industries Processes Application Procedures Additives/Extenders Specialties Future Developments Commercial Uses: Compounding and Formulating www.entrepreneurindia.co Chemical Intermediates Adhesives Agricultural Formulations Cellophane Film Humectants Cosmetics and Toiletries Detergents and Cleaners Inks Paints and Coatings Pharmaceutical Products Rubber Compounds Miscellaneous Products Cork Products Food Products Lubricants and Hydraulic Fluids Paper Products www.entrepreneurindia.co Photographic Developers Sponges Wood swelling agent Commercial Uses: for Processing Aids Ceramics Dialysis Operations Electroplating Heat Transfer Baths Leather Treatment Metal Working Operations Paper Products Petroleum Recovery and Processing Plastic Compounding Rubber Products Textile Products Wood Products www.entrepreneurindia.co Industries Using Polyethylene Glycols Adhesives Agricultural Products Ceramics Products Chemical Specialties Cosmetics and Toiletries Electronic and Electrowinning Food Products Inks and Printing Leather Processing Lubricants and Hydraulic Fluids Medical Sundries Metal Fabricating Packaging Materials Paints and Coatings Paper Products www.entrepreneurindia.co Petroleum Recovery and Processing Pharmaceuticals Photographic Products Plastics Products Rubber and Elastomers Textile Products Wood Processing Formulations Fatty Acid Esters Water Dispersible Alkyd Resin for Paints Suppository Bases Ointment Bases Cosmetic Cream Hand Lotion Brushless Shaving Cream www.entrepreneurindia.co Cream Rouge (Vanishing) Perfume Stick Clay Starch Paper Coating Metal Working Lubricant Ball point Pen Ink Laboratory Techniques Identification of PEGs Determination of PEGs in Other Materials

1 6. ALGINATE POLY ETHYLENE OXIDE Chemical Nature Narrow Molecular Weight Distribution Grades Hydrogels Thermoplastic Compound Hydrodynamic Drag Reduction Slurry www.entrepreneurindia.co Oxidative Degradation Association Complexes Physical Properties Bulk Properties Manufacture Biological/Toxicological Properties Toxicological Studies Biodegradability Rheological properties Viscosity Additives/Extenders Applications Application procedures Boiling Water Dispersion Nonsolvent Dispersion www.entrepreneurindia.co Commercial Uses: Compounding and Formulating Adhesives Water Soluble Paper Adhesives Adhesives from Association Complexes Industrial Supplies Thickened Cleaning Solutions Construction Products Paving Composition Water Soluble Purge Dam Paints and Paint Removers Latex Paints Spatter Finish Thickener for Paint and Varnish Remover Pharmaceuticals Dispersant for Calamine Lotion www.entrepreneurindia.co Rubbing Alcohol Printing Products Microencapsulated Inks Lithographic Press Dampening Fluid Soap, Detergents, and Personal Care Products Detergents Toothpastes Denture Fixative Shaving Stick Ophthalmic Solution Absorbent Pads Water Soluble Films Seed Tape Water Soluble Packaging Commercial Uses: Processing Aids www.entrepreneurindia.co Binder Ceramics Battery Electrodes Fluorescent Lamps Soil Stabilization Other Binder Applications Coatings and Sizes Tablet Coatings Glass Fiber Size Dispersant Vinyl Polymerization Glass Fiber Reinforced Concrete Flocculation Clays Coal Silica www.entrepreneurindia.co Filier Retention Drainage Aid (Paper Making) Hydrodynamic Drag Reduction Fire fighting Additive Fluid jet Cutting Additive to Prevent Sewer Surcharges Other Drag Reduction Applications Thermoplastics Manufacture Textile Antistat Fugitive Textile Weft Thickening / Rheology Control Antimist Additive Drift Control Additive Oil Recovery Fluids Water Retention Asbestos Cement Extrusion Aid Soil Amendment www.entrepreneurindia.co Industries Using Poly (Ethylene Oxide) Formulations Aluminum and Metal Cleaner Calamine Lotion Denture Fixative, Powder Detergent Bars Detergent Liquid Lithographic Press Dampening Fluid Microencapsulation Paint and Varnish Remover Thickened Acetic Acid Thickened Hydrochloric Acid (Muriatric Acid) Thickened Sulfuric Acid Rubber Lubricant (for Mounting of Tires) Toothpastes www.entrepreneurindia.co 1 7. POLYVINYLPYRROLIDONE General Information Chemical Nature Physical Properties Manufacture Rheological Properties Intrinsic Viscosity Toxicological Properties General Acute Toxicology National Cancer Institute Sub acute and Chronic PVP Films Compatibilities Future Developments Applications of PVP www.entrepreneurindia.co Pharmacy Medicine Beverages Cosmetics and Toiletries Textiles Paper Adhesives Detergents and Soaps Polymers and Polymerization Agricultural Photography and Lithography

1 8. SILICONES RESINS Chlorosilanes Commercial Production of Monomeric Intermediates www.entrepreneurindia.co Silicone Fluids Manufacture Properties and Uses Thermal Stability Rheological Characteristics Surface Activity Lubricating Properties Electrical Properties Other Characteristics Identification Silicone Elastomers Manufacture of Base Polymers Fillers Processing Vulcanization Properties and Uses www.entrepreneurindia.co High and Low Temperature Applications Electrical Applications Molding and Mold Release Applications Thermal Insulation and Ablative Applications Construction Products Medical Applications Convenience Uses and Miscellaneous Applications Silicone Resins Manufacture Cure Properties and Uses Greases and Compounds Surfactants Primers and Adhesion Promoters Preparation & Formulation of Silicone Resin Based Coatings Cure Catalyst Driers www.entrepreneurindia.co Pigments and Dyes Thinners Formulations Application Guides Surface Preparation Priming Applying the Coating Curing Surfactants and Specialties Methods of Manufacture Properties Emulsions

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